C₂₄H₂₃ClFN₅O₄

Base Information

Chemical Name:C₂₄H₂₃ClFN₅O₄
CAS No.:1466514-32-8
Molecular Formula:C₂₄H₂₃ClFN₅O₄
Molecular Weight:499.929
Hs Code.:

C<sub>24</sub>H<sub>23</sub>ClFN<sub>5</sub>O<sub>4</sub>

Synonyms:C₂₄H₂₃ClFN₅O₄

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Chemical Property of C₂₄H₂₃ClFN₅O₄

Chemical Property:

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Technology Process of C₂₄H₂₃ClFN₅O₄

There total 11 articles about C₂₄H₂₃ClFN₅O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1466514-96-4
C₂₀H₁₇ClN₄O₅

: 1427379-42-7
3-fluoro-3-methylazetidine hydrochloride

: 1466514-32-8
C₂₄H₂₃ClFN₅O₄

Guidance literature:: With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 20 ℃; for 15h;

Reference yield:

: 884004-48-2
2-amino-4-chloronicotinaldehyde

: 1466514-32-8
C₂₄H₂₃ClFN₅O₄

Guidance literature:: Multi-step reaction with 6 steps

1: N-Bromosuccinimide / 1,2-dichloro-ethane / 1 h / Reflux

2: titanium tetrachloride / tetrahydrofuran; dichloromethane / 41.5 h / 0 - 20 °C

3: potassium carbonate / N,N-dimethyl-formamide / 3.5 h / 20 °C

4: palladium diacetate; ruphos; caesium carbonate / 1,4-dioxane / 0.67 h / 120 °C / Inert atmosphere; Microwave irradiation

5: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

6: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 15 h / 20 °C

With N-Bromosuccinimide; palladium diacetate; titanium tetrachloride; potassium carbonate; caesium carbonate; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; ruphos; In tetrahydrofuran; 1,4-dioxane; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

Reference yield:

: 104-86-9
4-chlorobenzylamine

: 1466514-32-8
C₂₄H₂₃ClFN₅O₄

Guidance literature:: Multi-step reaction with 6 steps

1: triethylamine / dichloromethane / 16.5 h / 0 - 20 °C

2: titanium tetrachloride / tetrahydrofuran; dichloromethane / 41.5 h / 0 - 20 °C

3: potassium carbonate / N,N-dimethyl-formamide / 3.5 h / 20 °C

4: palladium diacetate; ruphos; caesium carbonate / 1,4-dioxane / 0.67 h / 120 °C / Inert atmosphere; Microwave irradiation

5: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

6: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 15 h / 20 °C

With palladium diacetate; titanium tetrachloride; potassium carbonate; caesium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; ruphos; In tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;