C₁₃H₁₇NSe

Base Information

• Chemical Name: C₁₃H₁₇NSe
• CAS No.: 1160556-75-1
• Molecular Formula: C₁₃H₁₇NSe
• Molecular Weight: 266.245
• Mol file: 1160556-75-1.mol

Synonyms:C₁₃H₁₇NSe

Chemical Property of C₁₃H₁₇NSe

Chemical Property:

Purity/Quality:

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Technology Process of C₁₃H₁₇NSe

There total 1 articles about C₁₃H₁₇NSe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

Isobutyronitrile (78-82-0) + 1-bromo-3-phenylselenopropane (118824-31-0) → C13H17NSe (1160556-75-1)

Guidance literature:

Isobutyronitrile; With lithium diisopropyl amide; In diethyl ether; hexane; at 0 ℃; for 1h;

1-bromo-3-phenylselenopropane; In diethyl ether; hexane; at 0 - 23 ℃; for 12h;

DOI:10.1021/ol900819u

Reference yield: 81.0%

C13H17NSe (1160556-75-1) → C13H18OSe (1160556-76-2)

Guidance literature:

C₁₃H₁₇NSe; With diisobutylaluminium hydride; In dichloromethane; toluene; at -78 ℃; for 1h;

With water; ammonium chloride; In dichloromethane; toluene;

DOI:10.1021/ol900819u

upstream raw materials:

Isobutyronitrile

1-bromo-3-phenylselenopropane

Downstream raw materials:

C₁₃H₁₈OSe

Refernces