N‐morpholinobenzenesulfonamide

Base Information

• Chemical Name: N‐morpholinobenzenesulfonamide
• CAS No.: 351186-42-0
• Molecular Formula: C₁₀H₁₄N₂O₃S
• Molecular Weight: 242.299
• Mol file: 351186-42-0.mol

Synonyms:N‐morpholinobenzenesulfonamide

Chemical Property of N‐morpholinobenzenesulfonamide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of N‐morpholinobenzenesulfonamide

There total 21 articles about N‐morpholinobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

1-aminomorpholine (4319-49-7) + diethoxydiphenylsilane (2553-19-7,155684-44-9) → N‐morpholinobenzenesulfonamide (351186-42-0)

Guidance literature:

With 1,4-diazabicyclo[2.2.2]octane-triethylenediamine-bis(sulfur dioxide); oxygen; copper diacetate; cesium fluoride; XPhos; In 1,4-dioxane; at 80 ℃;

DOI:10.1021/ol5018849

Reference yield: 98.0%

1-aminomorpholine (4319-49-7) + phenylboronic acid (98-80-6) → N‐morpholinobenzenesulfonamide (351186-42-0)

Guidance literature:

With DABCO-bis(sulfur dioxide); tetrabutylammomium bromide; oxygen; palladium diacetate; In 1,4-dioxane; at 80 ℃; for 12h;

DOI:10.1039/c2cc33725h

Reference yield: 97.0%

1-aminomorpholine (4319-49-7) + 3,3-diethyl-1-phenyltriaz-1-ene (13056-98-9) → N‐morpholinobenzenesulfonamide (351186-42-0)

Guidance literature:

With boron trifluoride diethyl etherate; sulfur dioxide; In acetonitrile; at 60 ℃; for 3h; Inert atmosphere; Schlenk technique;

DOI:10.1039/c4cc03481c

upstream raw materials:

1-aminomorpholine

iodobenzene

phenylboronic acid

benzenediazonium tetrafluoroborate

Downstream raw materials:

Benzyl phenyl sulfone

5-(2-(phenylsulfonyl)ethyl)-1H-indole