4-[2-(4-Chloro-phenyl)-benzo[1,3]dithiol-2-yl]-2-[2-(4-chloro-phenyl)-benzo[1,3]oxathiol-2-yl]-1H-pyrrole

Base Information

Chemical Name:4-[2-(4-Chloro-phenyl)-benzo[1,3]dithiol-2-yl]-2-[2-(4-chloro-phenyl)-benzo[1,3]oxathiol-2-yl]-1H-pyrrole
CAS No.:147089-35-8
Molecular Formula:C₃₀H₁₉Cl₂NOS₃
Molecular Weight:576.591
Hs Code.:

Synonyms:4-[2-(4-Chloro-phenyl)-benzo[1,3]dithiol-2-yl]-2-[2-(4-chloro-phenyl)-benzo[1,3]oxathiol-2-yl]-1H-pyrrole

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Chemical Property of 4-[2-(4-Chloro-phenyl)-benzo[1,3]dithiol-2-yl]-2-[2-(4-chloro-phenyl)-benzo[1,3]oxathiol-2-yl]-1H-pyrrole

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Technology Process of 4-[2-(4-Chloro-phenyl)-benzo[1,3]dithiol-2-yl]-2-[2-(4-chloro-phenyl)-benzo[1,3]oxathiol-2-yl]-1H-pyrrole

There total 4 articles about 4-[2-(4-Chloro-phenyl)-benzo[1,3]dithiol-2-yl]-2-[2-(4-chloro-phenyl)-benzo[1,3]oxathiol-2-yl]-1H-pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 58948-38-2
2-(4-Chlorophenyl)-1,3-benzoxathiolium tetrafluoroborate

: 147089-27-8
3-[2-(4-Chloro-phenyl)-benzo[1,3]dithiol-2-yl]-1H-pyrrole

: 147089-35-8
4-[2-(4-Chloro-phenyl)-benzo[1,3]dithiol-2-yl]-2-[2-(4-chloro-phenyl)-benzo[1,3]oxathiol-2-yl]-1H-pyrrole

Guidance literature:: With pyridine; In acetonitrile; for 0.5h; Ambient temperature;

Reference yield:

: 97188-31-3
(1-benzenesulfonyl-1H-pyrrol-3-yl)-(4-chlorophenyl)methanone

: 147089-35-8
4-[2-(4-Chloro-phenyl)-benzo[1,3]dithiol-2-yl]-2-[2-(4-chloro-phenyl)-benzo[1,3]oxathiol-2-yl]-1H-pyrrole

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / HBF₄-diethyl ether complex / benzene / Heating

2: 100 percent / 10percent aq. KOH / dioxane; methanol / 0.25 h / 50 °C

3: 96 percent / pyridine / acetonitrile / 0.5 h / Ambient temperature

With pyridine; tetrafluoroboric acid diethyl ether; potassium hydroxide; In 1,4-dioxane; methanol; acetonitrile; benzene;

Reference yield:

: 122-01-0
4-chloro-benzoyl chloride

: 147089-35-8
4-[2-(4-Chloro-phenyl)-benzo[1,3]dithiol-2-yl]-2-[2-(4-chloro-phenyl)-benzo[1,3]oxathiol-2-yl]-1H-pyrrole

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / anhydrous AlCl₃ / CH₂Cl₂ / 0.5 h / Ambient temperature

2: 100 percent / HBF₄-diethyl ether complex / benzene / Heating

3: 100 percent / 10percent aq. KOH / dioxane; methanol / 0.25 h / 50 °C

4: 96 percent / pyridine / acetonitrile / 0.5 h / Ambient temperature

With pyridine; tetrafluoroboric acid diethyl ether; potassium hydroxide; aluminium trichloride; In 1,4-dioxane; methanol; dichloromethane; acetonitrile; benzene;