(4-Chloro-phenyl)-{4-[2-(4-chloro-phenyl)-benzo[1,3]dithiol-2-yl]-1H-pyrrol-2-yl}-methanone

Base Information

Chemical Name:(4-Chloro-phenyl)-{4-[2-(4-chloro-phenyl)-benzo[1,3]dithiol-2-yl]-1H-pyrrol-2-yl}-methanone
CAS No.:147089-45-0
Molecular Formula:C₂₄H₁₅Cl₂NOS₂
Molecular Weight:468.427
Hs Code.:

Synonyms:(4-Chloro-phenyl)-{4-[2-(4-chloro-phenyl)-benzo[1,3]dithiol-2-yl]-1H-pyrrol-2-yl}-methanone

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Chemical Property of (4-Chloro-phenyl)-{4-[2-(4-chloro-phenyl)-benzo[1,3]dithiol-2-yl]-1H-pyrrol-2-yl}-methanone

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Technology Process of (4-Chloro-phenyl)-{4-[2-(4-chloro-phenyl)-benzo[1,3]dithiol-2-yl]-1H-pyrrol-2-yl}-methanone

There total 5 articles about (4-Chloro-phenyl)-{4-[2-(4-chloro-phenyl)-benzo[1,3]dithiol-2-yl]-1H-pyrrol-2-yl}-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 147089-35-8
4-[2-(4-Chloro-phenyl)-benzo[1,3]dithiol-2-yl]-2-[2-(4-chloro-phenyl)-benzo[1,3]oxathiol-2-yl]-1H-pyrrole

: 147089-45-0
(4-Chloro-phenyl)-{4-[2-(4-chloro-phenyl)-benzo[1,3]dithiol-2-yl]-1H-pyrrol-2-yl}-methanone

Guidance literature:: With tetrafluoroboric acid diethyl ether; In ethanol; for 3h; Ambient temperature;

Reference yield:

: 97188-31-3
(1-benzenesulfonyl-1H-pyrrol-3-yl)-(4-chlorophenyl)methanone

: 147089-45-0
(4-Chloro-phenyl)-{4-[2-(4-chloro-phenyl)-benzo[1,3]dithiol-2-yl]-1H-pyrrol-2-yl}-methanone

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / HBF₄-diethyl ether complex / benzene / Heating

2: 100 percent / 10percent aq. KOH / dioxane; methanol / 0.25 h / 50 °C

3: 96 percent / pyridine / acetonitrile / 0.5 h / Ambient temperature

4: 100 percent / HBF₄-diethyl ether complex / ethanol / 3 h / Ambient temperature

With pyridine; tetrafluoroboric acid diethyl ether; potassium hydroxide; In 1,4-dioxane; methanol; ethanol; acetonitrile; benzene;

Reference yield:

: 122-01-0
4-chloro-benzoyl chloride

: 147089-45-0
(4-Chloro-phenyl)-{4-[2-(4-chloro-phenyl)-benzo[1,3]dithiol-2-yl]-1H-pyrrol-2-yl}-methanone

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / anhydrous AlCl₃ / CH₂Cl₂ / 0.5 h / Ambient temperature

2: 100 percent / HBF₄-diethyl ether complex / benzene / Heating

3: 100 percent / 10percent aq. KOH / dioxane; methanol / 0.25 h / 50 °C

4: 96 percent / pyridine / acetonitrile / 0.5 h / Ambient temperature

5: 100 percent / HBF₄-diethyl ether complex / ethanol / 3 h / Ambient temperature

With pyridine; tetrafluoroboric acid diethyl ether; potassium hydroxide; aluminium trichloride; In 1,4-dioxane; methanol; ethanol; dichloromethane; acetonitrile; benzene;