4-chlorohydroxyiminomethyl-2-methyl-N-(2,2,2-trifluoroethyl)-benzoic acid amide

Base Information

• Chemical Name: 4-chlorohydroxyiminomethyl-2-methyl-N-(2,2,2-trifluoroethyl)-benzoic acid amide
• CAS No.: 864725-68-8
• Molecular Formula: C₁₁H₁₀ClF₃N₂O₂
• Molecular Weight: 294.661

Synonyms:4-chlorohydroxyiminomethyl-2-methyl-N-(2,2,2-trifluoroethyl)-benzoic acid amide

Chemical Property of 4-chlorohydroxyiminomethyl-2-methyl-N-(2,2,2-trifluoroethyl)-benzoic acid amide

Chemical Property:

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Technology Process of 4-chlorohydroxyiminomethyl-2-methyl-N-(2,2,2-trifluoroethyl)-benzoic acid amide

There total 1 articles about 4-chlorohydroxyiminomethyl-2-methyl-N-(2,2,2-trifluoroethyl)-benzoic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-hydroxyiminomethyl-2-methyl-N-(2,2,2-trifluoroethyl)-benzoic acid amide (864725-43-9) → 4-chlorohydroxyiminomethyl-2-methyl-N-(2,2,2-trifluoroethyl)-benzoic acid amide (864725-68-8)

Guidance literature:

With N-chloro-succinimide; In N,N-dimethyl-formamide; at 50 ℃; for 0.5h; Product distribution / selectivity;

Reference yield:

1,3-dichloro-5-(3,3,3-trifluoroprop-1-en-2-yl)benzene (864725-22-4) + 4-chlorohydroxyiminomethyl-2-methyl-N-(2,2,2-trifluoroethyl)-benzoic acid amide (864725-68-8) → 4-(5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazole-3-yl)-2-methyl-N-(2,2,2-trifluoroethyl)-benzoic acid amide

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 18h;

Reference yield:

3-bromodifluoromethoxy-1-(1-trifluoromethylethenyl)-benzene + 4-chlorohydroxyiminomethyl-2-methyl-N-(2,2,2-trifluoroethyl)-benzoic acid amide (864725-68-8) → 4-[5-(3-bromodifluoromethoxyphenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methyl-N-(2,2,2-trifluoroethyl)-benzoic acid amide

Guidance literature:

With potassium hydrogencarbonate; In 1,2-dimethoxyethane; at 20 ℃; for 18h;

upstream raw materials:

4-hydroxyiminomethyl-2-methyl-N-(2,2,2-trifluoroethyl)-benzoic acid amide

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