6'-trifluoroacetyl-2',3-diPNZ-1-(N-PNZ-4-amino-2(S)-hydroxy-butyryl)-3''-Boc-sisomicin

Base Information

Chemical Name:6'-trifluoroacetyl-2',3-diPNZ-1-(N-PNZ-4-amino-2(S)-hydroxy-butyryl)-3''-Boc-sisomicin
CAS No.:1154758-53-8
Molecular Formula:C₅₄H₆₆F₃N₉O₂₄
Molecular Weight:1282.16
Hs Code.:

Synonyms:6'-trifluoroacetyl-2',3-diPNZ-1-(N-PNZ-4-amino-2(S)-hydroxy-butyryl)-3''-Boc-sisomicin

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Chemical Property of 6'-trifluoroacetyl-2',3-diPNZ-1-(N-PNZ-4-amino-2(S)-hydroxy-butyryl)-3''-Boc-sisomicin

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Technology Process of 6'-trifluoroacetyl-2',3-diPNZ-1-(N-PNZ-4-amino-2(S)-hydroxy-butyryl)-3''-Boc-sisomicin

There total 8 articles about 6'-trifluoroacetyl-2',3-diPNZ-1-(N-PNZ-4-amino-2(S)-hydroxy-butyryl)-3''-Boc-sisomicin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1154758-50-5
6'-trifluoroacetyl-2',3-diPNZ-1-(N-PNZ-4-amino-2(S)-hydroxy-butyryl)-sisomicin

: 1154758-53-8
6'-trifluoroacetyl-2',3-diPNZ-1-(N-PNZ-4-amino-2(S)-hydroxy-butyryl)-3''-Boc-sisomicin

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In methanol; at 0 - 20 ℃;

Reference yield:

: 4457-32-3
4-nitrobenzyl chloroformate

: 1154758-53-8
6'-trifluoroacetyl-2',3-diPNZ-1-(N-PNZ-4-amino-2(S)-hydroxy-butyryl)-3''-Boc-sisomicin

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / tetrahydrofuran / 0 - 20 °C

2.1: zinc diacetate / methanol

2.2: 3 h

3.1: N,N-dimethyl-formamide

4.1: N-ethyl-N,N-diisopropylamine / methanol / 0 - 20 °C

With zinc diacetate; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;

Reference yield:

: 32385-11-8
sisomicin

: 1154758-53-8
6'-trifluoroacetyl-2',3-diPNZ-1-(N-PNZ-4-amino-2(S)-hydroxy-butyryl)-3''-Boc-sisomicin

Guidance literature:: Multi-step reaction with 3 steps

1.1: zinc diacetate / methanol

1.2: 3 h

2.1: N,N-dimethyl-formamide

3.1: N-ethyl-N,N-diisopropylamine / methanol / 0 - 20 °C

With zinc diacetate; N-ethyl-N,N-diisopropylamine; In methanol; N,N-dimethyl-formamide;