6'-trifluoroacetyl-2',3-diPNZ-1-(N-PNZ-4-amino-2(S)-hydroxy-butyryl)-sisomicin

Base Information

Chemical Name:6'-trifluoroacetyl-2',3-diPNZ-1-(N-PNZ-4-amino-2(S)-hydroxy-butyryl)-sisomicin
CAS No.:1154758-50-5
Molecular Formula:C₄₉H₅₈F₃N₉O₂₂
Molecular Weight:1182.04
Hs Code.:

Synonyms:6'-trifluoroacetyl-2',3-diPNZ-1-(N-PNZ-4-amino-2(S)-hydroxy-butyryl)-sisomicin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6'-trifluoroacetyl-2',3-diPNZ-1-(N-PNZ-4-amino-2(S)-hydroxy-butyryl)-sisomicin

Chemical Property:

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Technology Process of 6'-trifluoroacetyl-2',3-diPNZ-1-(N-PNZ-4-amino-2(S)-hydroxy-butyryl)-sisomicin

There total 7 articles about 6'-trifluoroacetyl-2',3-diPNZ-1-(N-PNZ-4-amino-2(S)-hydroxy-butyryl)-sisomicin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 149137-92-8
(2S)-4-(p-nitrobenzyloxycarbonyl)-amino-2-hydroxybutyric acid

: 1154758-32-3
6'-trifluoroacetyl-2',3-diPNZ-sisomicin

: 1154758-50-5
6'-trifluoroacetyl-2',3-diPNZ-1-(N-PNZ-4-amino-2(S)-hydroxy-butyryl)-sisomicin

Guidance literature:: (2S)-4-(p-nitrobenzyloxycarbonyl)-amino-2-hydroxybutyric acid; With N-hydroxy-5-norbomene-2,3-dicarboxylic acid imide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide;

6'-trifluoroacetyl-2',3-diPNZ-sisomicin; In N,N-dimethyl-formamide;

Reference yield:

: 1154758-37-8
(N-hydroxy-5-norbornene-2,3-dicarboxyl-imido)-N-PNZ-4-amino-2(S)-hydroxy-butanoate

: 1154758-32-3
6'-trifluoroacetyl-2',3-diPNZ-sisomicin

: 1154758-50-5
6'-trifluoroacetyl-2',3-diPNZ-1-(N-PNZ-4-amino-2(S)-hydroxy-butyryl)-sisomicin

Guidance literature:: In N,N-dimethyl-formamide;

Reference yield:

: 4457-32-3
4-nitrobenzyl chloroformate

: 1154758-50-5
6'-trifluoroacetyl-2',3-diPNZ-1-(N-PNZ-4-amino-2(S)-hydroxy-butyryl)-sisomicin

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / tetrahydrofuran / 0 - 20 °C

2.1: zinc diacetate / methanol

2.2: 3 h

3.1: N,N-dimethyl-formamide

With zinc diacetate; triethylamine; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;