(2S)-2-benzyloxycarbonylamino-5-oxo-heptanedioic acid 1-benzyl ester 6-ethyl ester

Base Information

Chemical Name:(2S)-2-benzyloxycarbonylamino-5-oxo-heptanedioic acid 1-benzyl ester 6-ethyl ester
CAS No.:608535-19-9
Molecular Formula:C₂₄H₂₇NO₇
Molecular Weight:441.481
Hs Code.:

Synonyms:(2S)-2-benzyloxycarbonylamino-5-oxo-heptanedioic acid 1-benzyl ester 6-ethyl ester

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Chemical Property of (2S)-2-benzyloxycarbonylamino-5-oxo-heptanedioic acid 1-benzyl ester 6-ethyl ester

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Technology Process of (2S)-2-benzyloxycarbonylamino-5-oxo-heptanedioic acid 1-benzyl ester 6-ethyl ester

There total 4 articles about (2S)-2-benzyloxycarbonylamino-5-oxo-heptanedioic acid 1-benzyl ester 6-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 3705-42-8
Cbz-(L)-Glu-OBn

: 6148-64-7
ethyl potassium malonate

: 608535-19-9
(2S)-2-benzyloxycarbonylamino-5-oxo-heptanedioic acid 1-benzyl ester 6-ethyl ester

Guidance literature:: Cbz-(L)-Glu-OBn; With 1,1'-carbonyldiimidazole; In tetrahydrofuran; at 25 ℃; for 1.5h; Inert atmosphere;

ethyl potassium malonate; With magnesium chloride; In tetrahydrofuran; at 25 ℃; for 14h; Inert atmosphere;
DOI:10.1021/jacs.5b01681

Reference yield: 95.0%

: 3705-42-8
Cbz-(L)-Glu-OBn

: 37517-78-5
magnesium bis(3-ethoxy-3-oxopropanoate)

: 608535-19-9
(2S)-2-benzyloxycarbonylamino-5-oxo-heptanedioic acid 1-benzyl ester 6-ethyl ester

Guidance literature:: Cbz-(L)-Glu-OBn; With 1,1'-carbonyldiimidazole; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;

magnesium bis(3-ethoxy-3-oxopropanoate); In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1039/c5ob02110c

Reference yield: 85.0%

: 3705-42-8
Cbz-(L)-Glu-OBn

: [3-ethoxy-3-hydroxyacrylato^(2-)-O¹O³]magnesate⁽²⁺⁾

: 608535-19-9
(2S)-2-benzyloxycarbonylamino-5-oxo-heptanedioic acid 1-benzyl ester 6-ethyl ester

Guidance literature:: Cbz-(L)-Glu-OBn; With 1,1'-carbonyldiimidazole; In tetrahydrofuran; at 20 ℃; for 2h;

[3-ethoxy-3-hydroxyacrylato^(2-)-O¹O³]magnesate⁽²⁺⁾; In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.1021/acs.orglett.7b00854