1-(2-methoxyethyl)-3-(2,3,4,5,6-pentamethylbenzyl)benzimidazolium chloride

Base Information

Chemical Name:1-(2-methoxyethyl)-3-(2,3,4,5,6-pentamethylbenzyl)benzimidazolium chloride
CAS No.:1239882-44-0
Molecular Formula:C₂₂H₂₉N₂O*Cl
Molecular Weight:372.938
Hs Code.:

Synonyms:1-(2-methoxyethyl)-3-(2,3,4,5,6-pentamethylbenzyl)benzimidazolium chloride

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Chemical Property of 1-(2-methoxyethyl)-3-(2,3,4,5,6-pentamethylbenzyl)benzimidazolium chloride

Chemical Property:

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Technology Process of 1-(2-methoxyethyl)-3-(2,3,4,5,6-pentamethylbenzyl)benzimidazolium chloride

There total 2 articles about 1-(2-methoxyethyl)-3-(2,3,4,5,6-pentamethylbenzyl)benzimidazolium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 484-65-1
2,3,4,5,6-pentamethylbenzyl chloride

: 118468-98-7
1-(2-methoxyethyl)-1H-benzo[d]imidazole

: 1239882-44-0
1-(2-methoxyethyl)-3-(2,3,4,5,6-pentamethylbenzyl)benzimidazolium chloride

Guidance literature:: In N,N-dimethyl-formamide; at 70 ℃;
DOI:10.1016/j.ica.2018.04.018

Reference yield:

: 51-17-2,79351-71-6
benzoimidazole

: 1239882-44-0
1-(2-methoxyethyl)-3-(2,3,4,5,6-pentamethylbenzyl)benzimidazolium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / Inert atmosphere; Reflux; Schlenk technique

2: N,N-dimethyl-formamide / 70 °C / Inert atmosphere; Schlenk technique

In ethanol; N,N-dimethyl-formamide;
DOI:10.1039/c8ra08897g