octakis(2,6-diethylphenyl)tetracyclo{4.1.0(1,5).0(2,6)}heptastannane

Base Information

Chemical Name:octakis(2,6-diethylphenyl)tetracyclo{4.1.0(1,5).0(2,6)}heptastannane
CAS No.:142979-29-1
Molecular Formula:C₈₀H₁₀₄Sn₇
Molecular Weight:1896.68
Hs Code.:

Synonyms:octakis(2,6-diethylphenyl)tetracyclo{4.1.0(1,5).0(2,6)}heptastannane

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Chemical Property of octakis(2,6-diethylphenyl)tetracyclo{4.1.0(1,5).0(2,6)}heptastannane

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Technology Process of octakis(2,6-diethylphenyl)tetracyclo{4.1.0(1,5).0(2,6)}heptastannane

There total 2 articles about octakis(2,6-diethylphenyl)tetracyclo{4.1.0(1,5).0(2,6)}heptastannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 84143-92-0
hexakis(2,6-diethylphenyl)cyclotristannane

: 108-88-3,15644-74-3,16713-13-6
toluene

: 122115-73-5
hexakis(2,6-diethylphenyl)pentastanna{1.1.1}propellane

: 142979-29-1
octakis(2,6-diethylphenyl)tetracyclo{4.1.0(1,5).0(2,6)}heptastannane

Guidance literature:: With Li; NH₄Cl; In tetrahydrofuran; addn. of freshly cut pieces of Li (5.22 mmol) to a suspension of (C6H3(C2H5)2)6Sn3 (0.87 mmol) in THF; stirring mixt. at room temp. for 18 h (react. is monitored by thin layer chromy.); removing excess Li by pipetting the THF soln. to a new flask;; addn. of solid NH4Cl, stirring mixt. at room temp. for 1 h; filtering, concg. filtrate in vac.; taking up residue in min. vol. of 7:1 hexane/toluene; chromy. (silica gel; hexane/toluene); elem. anal.; pptn. of C80H104Sn7 as toluene adduct;;
DOI:10.1021/ja00044a011

Reference yield:

: 84143-92-0
hexakis(2,6-diethylphenyl)cyclotristannane

: 142979-29-1
octakis(2,6-diethylphenyl)tetracyclo{4.1.0(1,5).0(2,6)}heptastannane

Guidance literature:: thermolysis;
DOI:10.1021/ja00044a011

Reference yield:

: 142979-29-1
octakis(2,6-diethylphenyl)tetracyclo{4.1.0(1,5).0(2,6)}heptastannane

: 23978-09-8
[2.2.2]cryptande

: {(C₆H₃(C₂H₅)2)8Sn₇}^(1-)*{K(C₁₈H₃₆N₂O₆)}⁽¹⁺⁾={(C₆H₃(C₂H₅)2)8Sn₇}{K(C₁₈H₃₆N₂O₆)}

Guidance literature:: With potassium amalgam; In tetrahydrofuran; placing (C6H3(C2H5)2)8Sn7 (0.005 mmol), C18H36N2O6 (0.005 mmol) and 0.1% potassium amalgam in quartz ESR tube equipped with ground glass joint; attaching tube to high vac. line and transferring THF (dried over K-mirror) to tube; sealing tube under vac.;; not isolated, detected by ESR;;
DOI:10.1021/ja00044a011