2-(4-chloro-phenyl)-3-cyclopropyl-1-(5-mercapto-[1,2,4]triazol-1-yl)-butan-2-ol

Base Information

• Chemical Name: 2-(4-chloro-phenyl)-3-cyclopropyl-1-(5-mercapto-[1,2,4]triazol-1-yl)-butan-2-ol
• CAS No.: 1258158-18-7
• Molecular Formula: C₁₅H₁₈ClN₃OS
• Molecular Weight: 323.846

Synonyms:2-(4-chloro-phenyl)-3-cyclopropyl-1-(5-mercapto-[1,2,4]triazol-1-yl)-butan-2-ol

Chemical Property of 2-(4-chloro-phenyl)-3-cyclopropyl-1-(5-mercapto-[1,2,4]triazol-1-yl)-butan-2-ol

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Technology Process of 2-(4-chloro-phenyl)-3-cyclopropyl-1-(5-mercapto-[1,2,4]triazol-1-yl)-butan-2-ol

There total 2 articles about 2-(4-chloro-phenyl)-3-cyclopropyl-1-(5-mercapto-[1,2,4]triazol-1-yl)-butan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

2-(4-chloro-phenyl)-3-cyclopropyl-1-(5-mercapto-[1,2,4]triazol-1-yl)-butan-2-ol (1258158-18-7) → 1-(2-(4-chlorophenyl)-3-cyclopropyl-2-hydroxybutyl)-1H-1,2,4-triazole-5(4H)-thione (1258158-18-7)

Guidance literature:

With sulfur; In N,N-dimethyl-formamide; at 190 ℃; for 72h;

Reference yield: 22.0%

1,2,4-Triazole (288-88-0) + 2-(4-chlorophenyl)-3-cyclopropyl-1,2-butylene oxide (94361-26-9) → 2-(4-chloro-phenyl)-3-cyclopropyl-1-(5-mercapto-[1,2,4]triazol-1-yl)-butan-2-ol (1258158-18-7)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 1.5h;

Reference yield: 94.0%

2-(4-chloro-phenyl)-3-cyclopropyl-1-(5-mercapto-[1,2,4]triazol-1-yl)-butan-2-ol (1258158-18-7) + methyl iodide (74-88-4) → 2-(4-chloro-phenyl)-3-cyclopropyl-1-(5-methylsulfanyl-[1,2,4]triazol-1-yl)-butan-2-ol (1258158-20-1)

Guidance literature:

With potassium carbonate; In acetonitrile; at 40 ℃; for 6h;

upstream raw materials:

1,2,4-Triazole

2-(4-chlorophenyl)-3-cyclopropyl-1,2-butylene oxide

Downstream raw materials:

2-(4-chloro-phenyl)-3-cyclopropyl-1-(5-methylcarbonylsulfanyl-[1,2,4]triazol-1-yl)-butan-2-ol

2-(4-chloro-phenyl)-3-cyclopropyl-1-(5-methylsulfanyl-[1,2,4]triazol-1-yl)-butan-2-ol

2-(4-chloro-phenyl)-3-cyclopropyl-1-(5-methoxycarbonylsulfanyl-[1,2,4]triazol-1-yl)-butan-2-ol

2-(2-chloro-phenyl)-1-(5-{2-[2-(2-chloro-phenyl)-3-cyclopropyl-2-hydroxy-butyl]-2H-[1,2,4]triazol-3-yldisulfanyl}-[1,2,4]triazol-1-yl)-3-cyclopropyl-butan-2-ol

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