2-Benzyl-3-phenyl-2-{[1-phenyl-meth-(E)-ylidene]-amino}-propionic acid ethyl ester

Base Information

• Chemical Name: 2-Benzyl-3-phenyl-2-{[1-phenyl-meth-(E)-ylidene]-amino}-propionic acid ethyl ester
• CAS No.: 99330-18-4
• Molecular Formula: C₂₅H₂₅NO₂
• Molecular Weight: 371.479

Synonyms:2-Benzyl-3-phenyl-2-{[1-phenyl-meth-(E)-ylidene]-amino}-propionic acid ethyl ester

Chemical Property of 2-Benzyl-3-phenyl-2-{[1-phenyl-meth-(E)-ylidene]-amino}-propionic acid ethyl ester

Chemical Property:

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Technology Process of 2-Benzyl-3-phenyl-2-{[1-phenyl-meth-(E)-ylidene]-amino}-propionic acid ethyl ester

There total 2 articles about 2-Benzyl-3-phenyl-2-{[1-phenyl-meth-(E)-ylidene]-amino}-propionic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

benzyl chloride (100-44-7) + (S)-3-Phenyl-2-{[1-phenyl-meth-(E)-ylidene]-amino}-propionic acid ethyl ester (78843-66-0,118110-66-0,137967-42-1) → 2-Benzyl-3-phenyl-2-{[1-phenyl-meth-(E)-ylidene]-amino}-propionic acid ethyl ester (99330-18-4)

Guidance literature:

With potassium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In acetonitrile; for 8h; Ambient temperature;

DOI:10.1016/S0040-4020(01)86041-5

Reference yield:

ethyl N-benzylideneglycinate (40682-54-0) → 2-Benzyl-3-phenyl-2-{[1-phenyl-meth-(E)-ylidene]-amino}-propionic acid ethyl ester (99330-18-4)

Guidance literature:

With potassium tert-butylate; In tetrahydrofuran; at 0 - 20 ℃; for 1h;

DOI:10.1002/ejoc.200800907

Reference yield:

2-Benzyl-3-phenyl-2-{[1-phenyl-meth-(E)-ylidene]-amino}-propionic acid ethyl ester (99330-18-4) → ethyl 2-amino-2-benzyl-3-phenylpropanoate (93949-90-7)

Guidance literature:

With hydrogenchloride; water; In tetrahydrofuran; for 4h;

DOI:10.1002/ejoc.200800907

upstream raw materials:

benzyl chloride

(S)-3-Phenyl-2-{[1-phenyl-meth-(E)-ylidene]-amino}-propionic acid ethyl ester

ethyl N-benzylideneglycinate

Downstream raw materials:

2-amino-2-benzyl-3-phenylpropanoic acid

ethyl 2-amino-2-benzyl-3-phenylpropanoate

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