4-phenylbutanoic peroxyanhydride

Base Information

Chemical Name:4-phenylbutanoic peroxyanhydride
CAS No.:52565-60-3
Molecular Formula:C₂₀H₂₂O₄
Molecular Weight:326.392
Hs Code.:

Synonyms:4-phenylbutanoic peroxyanhydride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-phenylbutanoic peroxyanhydride

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Technology Process of 4-phenylbutanoic peroxyanhydride

There total 2 articles about 4-phenylbutanoic peroxyanhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 18496-54-3
phenylbutyric acid chloride

: 52565-60-3
4-phenylbutanoic peroxyanhydride

Guidance literature:: With pyridine; dihydrogen peroxide; In diethyl ether; water; for 2h; Inert atmosphere;
DOI:10.1021/acs.orglett.5b03399

Reference yield: 39.0%

: 1821-12-1
4-Phenylbutyric acid

: 52565-60-3
4-phenylbutanoic peroxyanhydride

Guidance literature:: 4-Phenylbutyric acid; With dmap; dihydrogen peroxide; In dichloromethane; water; at 0 ℃; for 0.166667h; Inert atmosphere;

With dicyclohexyl-carbodiimide; In dichloromethane; water; at 0 ℃; for 3.5h; Inert atmosphere;
DOI:10.1021/ja211679v

Reference yield: 89.0%

: 3033-80-5
8-methoxy-2-methylquinoline

: 52565-60-3
4-phenylbutanoic peroxyanhydride

: 8-methoxy-2-methyl-4-(3-phenylpropyl)quinoline

Guidance literature:: With trifluorormethanesulfonic acid; In acetonitrile; at 80 ℃; for 12h; Inert atmosphere; Schlenk technique;
DOI:10.1055/s-0037-1609965