methyl 4-acetamido-3-(benzyloxy)-6-(4-chloro-2-fluoro-3-methoxyphenyl)picolinate

Base Information

Chemical Name:methyl 4-acetamido-3-(benzyloxy)-6-(4-chloro-2-fluoro-3-methoxyphenyl)picolinate
CAS No.:1417332-47-8
Molecular Formula:C₂₃H₂₀ClFN₂O₅
Molecular Weight:458.874
Hs Code.:

Synonyms:methyl 4-acetamido-3-(benzyloxy)-6-(4-chloro-2-fluoro-3-methoxyphenyl)picolinate

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Chemical Property of methyl 4-acetamido-3-(benzyloxy)-6-(4-chloro-2-fluoro-3-methoxyphenyl)picolinate

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Technology Process of methyl 4-acetamido-3-(benzyloxy)-6-(4-chloro-2-fluoro-3-methoxyphenyl)picolinate

There total 1 articles about methyl 4-acetamido-3-(benzyloxy)-6-(4-chloro-2-fluoro-3-methoxyphenyl)picolinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 851442-71-2
4-acetylamino-3-benzyloxy-6-bromo-pyridine-2-carboxylic acid methyl ester

: 944129-07-1
(4-chloro-2-fluoro-3-methoxyphenyl)-boronic acid

: 1417332-47-8
methyl 4-acetamido-3-(benzyloxy)-6-(4-chloro-2-fluoro-3-methoxyphenyl)picolinate

Guidance literature:: With cesium fluoride; bis-triphenylphosphine-palladium(II) chloride; In 1,2-dimethoxyethane; water; at 100 ℃; for 0.25h; microwave irradiation;

Reference yield:

: 1417332-47-8
methyl 4-acetamido-3-(benzyloxy)-6-(4-chloro-2-fluoro-3-methoxyphenyl)picolinate

: 1417332-44-5
methyl 4-acetamido-6-(4-chloro-2-fluoro-3-methoxyphenyl)-3-hydroxypicolinate

Guidance literature:: With hydrogen; 10 wt% Pd(OH)2 on carbon; In ethanol; for 24h;

Reference yield:

: 1417332-47-8
methyl 4-acetamido-3-(benzyloxy)-6-(4-chloro-2-fluoro-3-methoxyphenyl)picolinate

: 1417331-18-0
methyl 4-acetamido-6-(4-chloro-2-fluoro-3-methoxyphenyl)-3-methoxypicolinate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / 10 wt% Pd(OH)2 on carbon / ethanol / 24 h

2: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 24 h

With hydrogen; triphenylphosphine; diethylazodicarboxylate; 10 wt% Pd(OH)2 on carbon; In tetrahydrofuran; ethanol;