methyl 4-acetamido-6-(4-chloro-2-fluoro-3-methoxyphenyl)-3-hydroxypicolinate

Base Information

Chemical Name:methyl 4-acetamido-6-(4-chloro-2-fluoro-3-methoxyphenyl)-3-hydroxypicolinate
CAS No.:1417332-44-5
Molecular Formula:C₁₆H₁₄ClFN₂O₅
Molecular Weight:368.749
Hs Code.:

Synonyms:methyl 4-acetamido-6-(4-chloro-2-fluoro-3-methoxyphenyl)-3-hydroxypicolinate

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Chemical Property of methyl 4-acetamido-6-(4-chloro-2-fluoro-3-methoxyphenyl)-3-hydroxypicolinate

Chemical Property:

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Technology Process of methyl 4-acetamido-6-(4-chloro-2-fluoro-3-methoxyphenyl)-3-hydroxypicolinate

There total 3 articles about methyl 4-acetamido-6-(4-chloro-2-fluoro-3-methoxyphenyl)-3-hydroxypicolinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1417332-47-8
methyl 4-acetamido-3-(benzyloxy)-6-(4-chloro-2-fluoro-3-methoxyphenyl)picolinate

: 1417332-44-5
methyl 4-acetamido-6-(4-chloro-2-fluoro-3-methoxyphenyl)-3-hydroxypicolinate

Guidance literature:: With hydrogen; 10 wt% Pd(OH)2 on carbon; In ethanol; for 24h;

Reference yield:

: 851442-71-2
4-acetylamino-3-benzyloxy-6-bromo-pyridine-2-carboxylic acid methyl ester

: 1417332-44-5
methyl 4-acetamido-6-(4-chloro-2-fluoro-3-methoxyphenyl)-3-hydroxypicolinate

Guidance literature:: Multi-step reaction with 2 steps

1: cesium fluoride / bis-triphenylphosphine-palladium(II) chloride / 1,2-dimethoxyethane; water / 0.25 h / 100 °C / microwave irradiation

2: hydrogen / 10 wt% Pd(OH)2 on carbon / ethanol / 24 h

With hydrogen; cesium fluoride; bis-triphenylphosphine-palladium(II) chloride; 10 wt% Pd(OH)2 on carbon; In 1,2-dimethoxyethane; ethanol; water;

Reference yield:

: 944129-07-1
(4-chloro-2-fluoro-3-methoxyphenyl)-boronic acid

: 1417332-44-5
methyl 4-acetamido-6-(4-chloro-2-fluoro-3-methoxyphenyl)-3-hydroxypicolinate

Guidance literature:: Multi-step reaction with 2 steps

1: cesium fluoride / bis-triphenylphosphine-palladium(II) chloride / 1,2-dimethoxyethane; water / 0.25 h / 100 °C / microwave irradiation

2: hydrogen / 10 wt% Pd(OH)2 on carbon / ethanol / 24 h

With hydrogen; cesium fluoride; bis-triphenylphosphine-palladium(II) chloride; 10 wt% Pd(OH)2 on carbon; In 1,2-dimethoxyethane; ethanol; water;