5-methyl-3-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-1-tosyl-1,2,4-triazole

Base Information

Chemical Name:5-methyl-3-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-1-tosyl-1,2,4-triazole
CAS No.:1430730-65-6
Molecular Formula:C₄₄H₃₇N₃O₁₁S
Molecular Weight:815.857
Hs Code.:

Synonyms:5-methyl-3-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-1-tosyl-1,2,4-triazole

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Chemical Property of 5-methyl-3-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-1-tosyl-1,2,4-triazole

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Technology Process of 5-methyl-3-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-1-tosyl-1,2,4-triazole

There total 6 articles about 5-methyl-3-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-1-tosyl-1,2,4-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1430730-32-7
N¹-tosyl-C-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)formamidrazone

: 75-36-5
acetyl chloride

: 1430730-65-6
5-methyl-3-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-1-tosyl-1,2,4-triazole

Guidance literature:: With pyridine; In chloroform; at 0 - 20 ℃; for 48h;
DOI:10.1021/ml4001529

Reference yield: 63.0%

: N-acetyl-C-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)thioformamide

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 1430730-65-6
5-methyl-3-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-1-tosyl-1,2,4-triazole

Guidance literature:: With pyridine; at 20 ℃; for 2h; regioselective reaction;
DOI:10.1016/j.tet.2017.05.014

Reference yield:

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 1430730-65-6
5-methyl-3-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-1-tosyl-1,2,4-triazole

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 72 h / 20 °C

2: pyridine / chloroform / 0.25 h / 20 °C / Cooling with ice

With pyridine; In dichloromethane; chloroform;