phenethyl 2-methoxypyridin-4-ylcarbamate

Base Information

Chemical Name:phenethyl 2-methoxypyridin-4-ylcarbamate
CAS No.:1580503-87-2
Molecular Formula:C₁₅H₁₆N₂O₃
Molecular Weight:272.304
Hs Code.:

Synonyms:phenethyl 2-methoxypyridin-4-ylcarbamate

Suppliers and Price of phenethyl 2-methoxypyridin-4-ylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of phenethyl 2-methoxypyridin-4-ylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of phenethyl 2-methoxypyridin-4-ylcarbamate

There total 2 articles about phenethyl 2-methoxypyridin-4-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 201230-82-2
carbon monoxide

: 60-12-8
2-phenylethanol

: 1556227-58-7
4-azido-2-methoxypyridine

: 1580503-87-2
phenethyl 2-methoxypyridin-4-ylcarbamate

Guidance literature:: With triethylamine; palladium dichloride; In N,N-dimethyl acetamide; at 70 ℃; for 24h; under 760.051 Torr; Schlenk technique;
DOI:10.1039/c4cc00538d

Reference yield:

: 20265-39-8
4-amino-2-methoxypyridine

: 1580503-87-2
phenethyl 2-methoxypyridin-4-ylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / water / 0 °C

1.2: 0.17 h

2.1: palladium dichloride; triethylamine / N,N-dimethyl acetamide / 24 h / 70 °C / 760.05 Torr / Schlenk technique

With hydrogenchloride; triethylamine; palladium dichloride; In N,N-dimethyl acetamide; water;
DOI:10.1039/c4cc00538d