(1-(2-N,N-dimethylamino)-ethylene-3-mesityl)imidazolium chloride hydrochloride

Base Information

• Chemical Name: (1-(2-N,N-dimethylamino)-ethylene-3-mesityl)imidazolium chloride hydrochloride
• CAS No.: 1210866-46-8
• Molecular Formula: C₁₆H₂₄N₃*ClH*Cl
• Molecular Weight: 330.301
• Mol file: 1210866-46-8.mol

Synonyms:(1-(2-N,N-dimethylamino)-ethylene-3-mesityl)imidazolium chloride hydrochloride

Chemical Property of (1-(2-N,N-dimethylamino)-ethylene-3-mesityl)imidazolium chloride hydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of (1-(2-N,N-dimethylamino)-ethylene-3-mesityl)imidazolium chloride hydrochloride

There total 1 articles about (1-(2-N,N-dimethylamino)-ethylene-3-mesityl)imidazolium chloride hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

(2-chloroethyl)dimethylamine hydrochloride (4584-46-7) + N-(2,4,6-trimethylphenyl)imidazole (25364-44-7) → (1-(2-N,N-dimethylamino)-ethylene-3-mesityl)imidazolium chloride hydrochloride (1210866-46-8)

Guidance literature:

In acetonitrile; for 72h; Reflux;

DOI:10.1039/c5cc07455j

Reference yield: 99.0%

(1-(2-N,N-dimethylamino)-ethylene-3-mesityl)imidazolium chloride hydrochloride (1210866-46-8) + silver(l) oxide (20667-12-3) → bis[(1-(2-N,N-dimethylamino)-ethylene-3-mesityl)imidazol-2-ylidene] disilver(I) dichloride

Guidance literature:

In dichloromethane; byproducts: AgCl; Ag2O and imidazolium salt suspended in CH2Cl2; stirred at room temp. overnight; modified from H. M. J. Wang, I. J. B. Lin, Organometallics, 1998, 17, 972; filtered over Celite; washed with CH2Cl2; filtrate concd.;

DOI:10.1039/b906817a

Reference yield: 90.0%

(1-(2-N,N-dimethylamino)-ethylene-3-mesityl)imidazolium chloride hydrochloride (1210866-46-8) → 3-(2-(dimethylamino)ethyl)-1-mesityl-1H-imidazol-3-ium chloride (1192215-59-0)

Guidance literature:

With sodium hydroxide; In methanol; at 20 ℃; for 1h;

DOI:10.1039/c5cc07455j

upstream raw materials:

(2-chloroethyl)dimethylamine hydrochloride

N-(2,4,6-trimethylphenyl)imidazole

Downstream raw materials:

3-(2-(dimethylamino)ethyl)-1-mesityl-1H-imidazol-3-ium chloride