C₁₅H₁₆ClNO₂

Base Information

Chemical Name:C₁₅H₁₆ClNO₂
CAS No.:1349798-37-3
Molecular Formula:C₁₅H₁₆ClNO₂
Molecular Weight:277.751
Hs Code.:

C<sub>15</sub>H<sub>16</sub>ClNO<sub>2</sub>

Synonyms:C₁₅H₁₆ClNO₂

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Chemical Property of C₁₅H₁₆ClNO₂

Chemical Property:

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Technology Process of C₁₅H₁₆ClNO₂

There total 3 articles about C₁₅H₁₆ClNO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1349798-36-2
C₁₂H₁₁NO₂

: 109-70-6
1.3-chlorobromopropane

: 1349798-37-3
C₁₅H₁₆ClNO₂

Guidance literature:: With potassium carbonate; In acetonitrile; at 80 ℃; for 24h;
DOI:10.1016/j.bmcl.2011.09.091

Reference yield:

: 81971-39-3
5-bromo-1-methylpyridin-2(1H)-one

: 1349798-37-3
C₁₅H₁₆ClNO₂

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; lithium chloride / ethanol; water; toluene / 5 h / 100 °C

2: potassium carbonate / acetonitrile / 24 h / 80 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; potassium carbonate; lithium chloride; In ethanol; water; toluene; acetonitrile; 1: Suzuki coupling;
DOI:10.1016/j.bmcl.2011.09.091

Reference yield:

: 13466-38-1,49843-23-4
5-bromopyridin-2(1H)-one

: 1349798-37-3
C₁₅H₁₆ClNO₂

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / dimethyl sulfoxide / 20 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; lithium chloride / ethanol; water; toluene / 5 h / 100 °C

3: potassium carbonate / acetonitrile / 24 h / 80 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; potassium carbonate; lithium chloride; In ethanol; water; dimethyl sulfoxide; toluene; acetonitrile; 2: Suzuki coupling;
DOI:10.1016/j.bmcl.2011.09.091