(1R,2S,5R)-2-{1-[((S)-1,3-Dimethyl-but-2-enyl)-(2-phenylselanyl-ethyl)-amino]-1-methyl-ethyl}-5-methyl-cyclohexanol

Base Information

Chemical Name:(1R,2S,5R)-2-{1-[((S)-1,3-Dimethyl-but-2-enyl)-(2-phenylselanyl-ethyl)-amino]-1-methyl-ethyl}-5-methyl-cyclohexanol
CAS No.:323999-97-9
Molecular Formula:C₂₄H₃₉NOSe
Molecular Weight:436.54
Hs Code.:

Synonyms:(1R,2S,5R)-2-{1-[((S)-1,3-Dimethyl-but-2-enyl)-(2-phenylselanyl-ethyl)-amino]-1-methyl-ethyl}-5-methyl-cyclohexanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2S,5R)-2-{1-[((S)-1,3-Dimethyl-but-2-enyl)-(2-phenylselanyl-ethyl)-amino]-1-methyl-ethyl}-5-methyl-cyclohexanol

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Technology Process of (1R,2S,5R)-2-{1-[((S)-1,3-Dimethyl-but-2-enyl)-(2-phenylselanyl-ethyl)-amino]-1-methyl-ethyl}-5-methyl-cyclohexanol

There total 1 articles about (1R,2S,5R)-2-{1-[((S)-1,3-Dimethyl-but-2-enyl)-(2-phenylselanyl-ethyl)-amino]-1-methyl-ethyl}-5-methyl-cyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 917-64-6
methyl magnesium iodide

: 235093-69-3
N-(phenylseleno)ethyl-2α-(2',2'-dimethylvinyl)-4,4,7α-trimethyl-trans-octahydro-1,3-benzoxazine

: 323999-97-9
(1R,2S,5R)-2-{1-[((S)-1,3-Dimethyl-but-2-enyl)-(2-phenylselanyl-ethyl)-amino]-1-methyl-ethyl}-5-methyl-cyclohexanol

Guidance literature:: In diethyl ether; at 20 ℃; for 1h;
DOI:10.1002/1099-0690(200011)2000:22<3727::AID-EJOC3727>3.0.CO;2-C

Reference yield: 98.0%

: 323999-97-9
(1R,2S,5R)-2-{1-[((S)-1,3-Dimethyl-but-2-enyl)-(2-phenylselanyl-ethyl)-amino]-1-methyl-ethyl}-5-methyl-cyclohexanol

: 323999-98-0
8-[(2'S,3'S)-3'-isopropyl-2'-methylpyrrolidinyl] menthol

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; Heating;
DOI:10.1002/1099-0690(200011)2000:22<3727::AID-EJOC3727>3.0.CO;2-C

Reference yield:

: 323999-97-9
(1R,2S,5R)-2-{1-[((S)-1,3-Dimethyl-but-2-enyl)-(2-phenylselanyl-ethyl)-amino]-1-methyl-ethyl}-5-methyl-cyclohexanol

: 89-82-7,90449-51-7
pulegone

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / Bu₃SnH; AIBN / benzene / Heating

2: PCC; mol. sieves / CH₂Cl₂ / 2 h / 20 °C

3: KOH; water / tetrahydrofuran; methanol / 2 h

With potassium hydroxide; molecular sieve; 2,2'-azobis(isobutyronitrile); water; tri-n-butyl-tin hydride; pyridinium chlorochromate; In tetrahydrofuran; methanol; dichloromethane; benzene;
DOI:10.1002/1099-0690(200011)2000:22<3727::AID-EJOC3727>3.0.CO;2-C