N-(1-bromo-8-oxo-5,6,7,8-tetrahydro-2-naphthalenyl)-2-fluorobenzenesulfonamide

Base Information

Chemical Name:N-(1-bromo-8-oxo-5,6,7,8-tetrahydro-2-naphthalenyl)-2-fluorobenzenesulfonamide
CAS No.:681246-83-3
Molecular Formula:C₁₆H₁₃BrFNO₃S
Molecular Weight:398.253
Hs Code.:

Synonyms:N-(1-bromo-8-oxo-5,6,7,8-tetrahydro-2-naphthalenyl)-2-fluorobenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(1-bromo-8-oxo-5,6,7,8-tetrahydro-2-naphthalenyl)-2-fluorobenzenesulfonamide

Chemical Property:

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Technology Process of N-(1-bromo-8-oxo-5,6,7,8-tetrahydro-2-naphthalenyl)-2-fluorobenzenesulfonamide

There total 1 articles about N-(1-bromo-8-oxo-5,6,7,8-tetrahydro-2-naphthalenyl)-2-fluorobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7-amino-8-bromo-3,4-dihydro-1(2H)-naphthalenone hydrobromide

: 2905-21-7
2-fluorobenzenesulfonyl chloride

: 681246-83-3
N-(1-bromo-8-oxo-5,6,7,8-tetrahydro-2-naphthalenyl)-2-fluorobenzenesulfonamide

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 24h;

Reference yield:

: 681246-83-3
N-(1-bromo-8-oxo-5,6,7,8-tetrahydro-2-naphthalenyl)-2-fluorobenzenesulfonamide

: 681247-02-9
N-(1-bromo-8-methylene-5,6,7,8-tetrahydro-2-naphthalenyl)-2-fluorobenzenesulfonamide

Guidance literature:: N-(1-bromo-8-oxo-5,6,7,8-tetrahydro-2-naphthalenyl)-2-fluorobenzenesulfonamide; With Tebbe reagent; In tetrahydrofuran; toluene; at 0 - 20 ℃;

With sodium hydroxide; In water;

Reference yield:

: 681246-83-3
N-(1-bromo-8-oxo-5,6,7,8-tetrahydro-2-naphthalenyl)-2-fluorobenzenesulfonamide

: 75-16-1
methylmagnesium bromide

: 681246-84-4
N-(1-bromo-8-methyl-5,6-dihydro-2-naphthalenyl)-2-fluorobenzenesulfonamide

Guidance literature:: N-(1-bromo-8-oxo-5,6,7,8-tetrahydro-2-naphthalenyl)-2-fluorobenzenesulfonamide; methylmagnesium bromide; In tetrahydrofuran; diethyl ether; at 70 ℃; for 4h;

With toluene-4-sulfonic acid; In toluene; at 110 ℃; for 1h;