1,3-O-di-propanoyl-4-benzylresorcinol

Base Information

• Chemical Name: 1,3-O-di-propanoyl-4-benzylresorcinol
• CAS No.: 960602-01-1
• Molecular Formula: C₁₉H₂₀O₄
• Molecular Weight: 312.365
• Mol file: 960602-01-1.mol

Synonyms:1,3-O-di-propanoyl-4-benzylresorcinol

Chemical Property of 1,3-O-di-propanoyl-4-benzylresorcinol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,3-O-di-propanoyl-4-benzylresorcinol

There total 2 articles about 1,3-O-di-propanoyl-4-benzylresorcinol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-benzylresorcinol (2284-30-2) + propionyl chloride (79-03-8) → 1,3-O-di-propanoyl-4-benzylresorcinol (960602-01-1)

Guidance literature:

With pyridine; at 20 ℃;

DOI:10.1016/j.tetlet.2007.09.104

Reference yield:

→ 1,3-O-di-propanoyl-4-benzylresorcinol (960602-01-1)

Guidance literature:

/BRN= 3379391/;

DOI:10.1002/ardp.19332710703

Reference yield: 100.0%

1,3-O-di-propanoyl-4-benzylresorcinol (960602-01-1) → 3-O-propanoyl-4-benzylresorcinol

Guidance literature:

With isopropyl alcohol; Candida antarctica lipase B; immobilized; In di-isopropyl ether; at 45 ℃; for 1h;

DOI:10.1016/j.tetlet.2007.09.104

upstream raw materials:

4-benzylresorcinol

propionyl chloride

Downstream raw materials:

4-benzylresorcinol

Refernces

• 1、 Miyazawa, Toshifumi,Hamada, Manabu,Morimoto, Ryohei,Maeda, Yuki. "Candida antarctica lipase B-mediated regioselective acylation of dihydroxybenzenes in organic solvents". . p. 3915 - 3923. Retrieved 2015/06/02.