N-(4-methoxybenzyl)-6,8-dimethyl-1H-pyrazolo[3',4':4,5]thieno[2,3-b]pyridin-3-amine

Base Information

Chemical Name:N-(4-methoxybenzyl)-6,8-dimethyl-1H-pyrazolo[3',4':4,5]thieno[2,3-b]pyridin-3-amine
CAS No.:1427790-09-7
Molecular Formula:C₁₈H₁₈N₄OS
Molecular Weight:338.433
Hs Code.:

Synonyms:N-(4-methoxybenzyl)-6,8-dimethyl-1H-pyrazolo[3',4':4,5]thieno[2,3-b]pyridin-3-amine

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Chemical Property of N-(4-methoxybenzyl)-6,8-dimethyl-1H-pyrazolo[3',4':4,5]thieno[2,3-b]pyridin-3-amine

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Technology Process of N-(4-methoxybenzyl)-6,8-dimethyl-1H-pyrazolo[3',4':4,5]thieno[2,3-b]pyridin-3-amine

There total 5 articles about N-(4-methoxybenzyl)-6,8-dimethyl-1H-pyrazolo[3',4':4,5]thieno[2,3-b]pyridin-3-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1427790-01-9
6,8-dimethyl-1H-pyrazolo[3',4':4,5]thieno[2,3-b]pyridin-3-amine

: 123-11-5
4-methoxy-benzaldehyde

: 1427790-09-7
N-(4-methoxybenzyl)-6,8-dimethyl-1H-pyrazolo[3',4':4,5]thieno[2,3-b]pyridin-3-amine

Guidance literature:: With sodium tris(acetoxy)borohydride; acetic acid; In 1,2-dichloro-ethane; for 1h;

Reference yield:

: 52505-57-4
3-Amino-4,6-dimethyl-thieno<2,3-b>pyridin-2-carbonitril

: 1427790-09-7
N-(4-methoxybenzyl)-6,8-dimethyl-1H-pyrazolo[3',4':4,5]thieno[2,3-b]pyridin-3-amine

Guidance literature:: Multi-step reaction with 3 steps

1: tert.-butylnitrite; copper(ll) bromide / acetonitrile / 1.5 h / 60 °C / Inert atmosphere

2: hydrazine / dimethyl sulfoxide / 0.17 h / 150 °C / Microwave irradiation; Sealed tube

3: sodium tris(acetoxy)borohydride; acetic acid / 1,2-dichloro-ethane / 1 h

With tert.-butylnitrite; sodium tris(acetoxy)borohydride; acetic acid; copper(ll) bromide; hydrazine; In dimethyl sulfoxide; 1,2-dichloro-ethane; acetonitrile;

Reference yield:

: 1427791-98-7
3-bromo-4,6-dimethylthieno[2,3-b]pyridine-2-carbonitrile

: 1427790-09-7
N-(4-methoxybenzyl)-6,8-dimethyl-1H-pyrazolo[3',4':4,5]thieno[2,3-b]pyridin-3-amine

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine / dimethyl sulfoxide / 0.17 h / 150 °C / Microwave irradiation; Sealed tube

2: sodium tris(acetoxy)borohydride; acetic acid / 1,2-dichloro-ethane / 1 h

With sodium tris(acetoxy)borohydride; acetic acid; hydrazine; In dimethyl sulfoxide; 1,2-dichloro-ethane;