5-(4-chlorophenyl)-2-(trifluoromethyl)-12-(4-(trifluoromethyl)phenyl)tetracene

Base Information

Chemical Name:5-(4-chlorophenyl)-2-(trifluoromethyl)-12-(4-(trifluoromethyl)phenyl)tetracene
CAS No.:1415646-21-7
Molecular Formula:C₃₂H₁₇ClF₆
Molecular Weight:550.93
Hs Code.:

Synonyms:5-(4-chlorophenyl)-2-(trifluoromethyl)-12-(4-(trifluoromethyl)phenyl)tetracene

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Chemical Property of 5-(4-chlorophenyl)-2-(trifluoromethyl)-12-(4-(trifluoromethyl)phenyl)tetracene

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Technology Process of 5-(4-chlorophenyl)-2-(trifluoromethyl)-12-(4-(trifluoromethyl)phenyl)tetracene

There total 3 articles about 5-(4-chlorophenyl)-2-(trifluoromethyl)-12-(4-(trifluoromethyl)phenyl)tetracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1,1'-(1,2-phenylene)bis(3-(4-(trifluoromethyl)phenyl)prop-2-yne-1,1-diyl)dimethyl dicarbonate

: 1679-18-1
4-Chlorophenylboronic acid

: 1415646-21-7
5-(4-chlorophenyl)-2-(trifluoromethyl)-12-(4-(trifluoromethyl)phenyl)tetracene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 50 ℃; Inert atmosphere;
DOI:10.1039/c2cc36700a

Reference yield:

: 705-31-7
4-trifluoromethylphenylacetylene

: 1415646-21-7
5-(4-chlorophenyl)-2-(trifluoromethyl)-12-(4-(trifluoromethyl)phenyl)tetracene

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: 1.5 h / 20 °C

2.1: pyridine; dmap / dichloromethane / 0 °C / Inert atmosphere

2.2: 2 h / 20 °C

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 50 °C / Inert atmosphere

With pyridine; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c2cc36700a

Reference yield:

: 1415646-42-2
1,1'-(1,2-phenylene)bis(3-(4-(trifluoromethyl)phenyl)prop-2-yn-1-ol)

: 1415646-21-7
5-(4-chlorophenyl)-2-(trifluoromethyl)-12-(4-(trifluoromethyl)phenyl)tetracene

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine; dmap / dichloromethane / 0 °C / Inert atmosphere

1.2: 2 h / 20 °C

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 50 °C / Inert atmosphere

With pyridine; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c2cc36700a