ethyl syn-7-chlorobicyclo<4.1.0>heptylacetate

Base Information

Chemical Name:ethyl syn-7-chlorobicyclo<4.1.0>heptylacetate
CAS No.:81652-62-2
Molecular Formula:C₁₁H₁₇ClO₂
Molecular Weight:216.708
Hs Code.:

Synonyms:ethyl syn-7-chlorobicyclo<4.1.0>heptylacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl syn-7-chlorobicyclo<4.1.0>heptylacetate

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Technology Process of ethyl syn-7-chlorobicyclo<4.1.0>heptylacetate

There total 2 articles about ethyl syn-7-chlorobicyclo<4.1.0>heptylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 823-69-8
7,7-dichloro-bicyclo[4.1.0]heptane

: 105-53-3
diethyl malonate

: 100-41-4,27536-89-6
ethylbenzene

: 81652-62-2
ethyl syn-7-chlorobicyclo<4.1.0>heptylacetate

: 81652-61-1
diethyl bicyclo<4.1.0>heptene-5-ylmalonate

: 81652-60-0
diethyl syn-7-chlorobicyclo<4.1.0>heptylmalonate

Guidance literature:: With 18-crown-6 ether; potassium tert-butylate; In dimethyl sulfoxide; at 45 - 50 ℃; for 30h; Yield given. Further byproducts given. Yields of byproduct given;
DOI:10.1016/S0040-4020(01)98899-4

Reference yield:

: 823-69-8
7,7-dichloro-bicyclo[4.1.0]heptane

: 105-53-3
diethyl malonate

: 611-14-3
2-Ethyltoluene

: 81652-63-3
ethyl bicyclo<4.1.0>heptene-5-ylacetate

: 81652-62-2
ethyl syn-7-chlorobicyclo<4.1.0>heptylacetate

: 81652-60-0
diethyl syn-7-chlorobicyclo<4.1.0>heptylmalonate

Guidance literature:: With potassium tert-butylate; In dimethyl sulfoxide; at 80 - 90 ℃; for 16h; Yield given. Further byproducts given. Yields of byproduct given;
DOI:10.1016/S0040-4020(01)98899-4