<4-Methoxy-benzoyl>malonsaeure-dinitril

Base Information

Chemical Name:<4-Methoxy-benzoyl>malonsaeure-dinitril
CAS No.:46407-88-9
Molecular Formula:C₁₁H₈N₂O₂
Molecular Weight:200.197
Hs Code.:

Synonyms:<4-Methoxy-benzoyl>malonsaeure-dinitril

Suppliers and Price of <4-Methoxy-benzoyl>malonsaeure-dinitril

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of <4-Methoxy-benzoyl>malonsaeure-dinitril

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of <4-Methoxy-benzoyl>malonsaeure-dinitril

There total 4 articles about <4-Methoxy-benzoyl>malonsaeure-dinitril which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 143-33-9,25596-52-5
sodium cyanide

: 100-06-1
1-(4-methoxyphenyl)ethanone

: 46407-88-9
<4-Methoxy-benzoyl>malonsaeure-dinitril

Guidance literature:: potassium iodide; In methanol; at 15 ℃; electrochemical oxidation; a constant current of 0.5 A; 10 F/mol of electrocity;
DOI:10.1021/jo00075a010

Reference yield:

: 100-07-2
4-methoxy-benzoyl chloride

: 109-77-3
malononitrile

: 46407-88-9
<4-Methoxy-benzoyl>malonsaeure-dinitril

Guidance literature:: With sodium hydride; In tetrahydrofuran; 1.) 5-10 deg C, 2.) room temp., 1h;
DOI:10.1039/P19960001545

Reference yield:

: 100-09-4
4-methoxybenzoic acid

: 46407-88-9
<4-Methoxy-benzoyl>malonsaeure-dinitril

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / Reflux

2: sodium hydride / tetrahydrofuran

With thionyl chloride; sodium hydride; In tetrahydrofuran;
DOI:10.2174/1570180811666140115234123