2,5-bis(dimethylcarbamoyl)-1-(4-methoxyphenyl)-1-pyrrole-3,4-diyl bis(2,2-dimethyl-3-(2-(2-(phosphonooxy)ethoxy)ethoxy)propanoate)

Base Information

Chemical Name:2,5-bis(dimethylcarbamoyl)-1-(4-methoxyphenyl)-1-pyrrole-3,4-diyl bis(2,2-dimethyl-3-(2-(2-(phosphonooxy)ethoxy)ethoxy)propanoate)
CAS No.:1443300-35-3
Molecular Formula:C₃₅H₅₅N₃O₁₉P₂
Molecular Weight:883.778
Hs Code.:

Synonyms:2,5-bis(dimethylcarbamoyl)-1-(4-methoxyphenyl)-1-pyrrole-3,4-diyl bis(2,2-dimethyl-3-(2-(2-(phosphonooxy)ethoxy)ethoxy)propanoate)

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Chemical Property of 2,5-bis(dimethylcarbamoyl)-1-(4-methoxyphenyl)-1-pyrrole-3,4-diyl bis(2,2-dimethyl-3-(2-(2-(phosphonooxy)ethoxy)ethoxy)propanoate)

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Technology Process of 2,5-bis(dimethylcarbamoyl)-1-(4-methoxyphenyl)-1-pyrrole-3,4-diyl bis(2,2-dimethyl-3-(2-(2-(phosphonooxy)ethoxy)ethoxy)propanoate)

There total 5 articles about 2,5-bis(dimethylcarbamoyl)-1-(4-methoxyphenyl)-1-pyrrole-3,4-diyl bis(2,2-dimethyl-3-(2-(2-(phosphonooxy)ethoxy)ethoxy)propanoate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1443300-67-1
2,5-bis(dimethylcarbamoyl)-1-(4-methoxyphenyl)-1H-pyrrole-3,4-diyl bis(3-(2-(2-((bis(benzyloxy)phosphoryl)oxy)ethoxy)ethoxy)-2,2-dimethylpropanoate)

: 1443300-35-3
2,5-bis(dimethylcarbamoyl)-1-(4-methoxyphenyl)-1-pyrrole-3,4-diyl bis(2,2-dimethyl-3-(2-(2-(phosphonooxy)ethoxy)ethoxy)propanoate)

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 45 ℃; under 7500.75 Torr;

Reference yield:

: 1443300-57-9
tert-butyl 3-(2-(2-((bis(benzyloxy)phosphoryl)oxy)ethoxy)ethoxy)-2,2-dimethylpropanoate

: 1443300-35-3
2,5-bis(dimethylcarbamoyl)-1-(4-methoxyphenyl)-1-pyrrole-3,4-diyl bis(2,2-dimethyl-3-(2-(2-(phosphonooxy)ethoxy)ethoxy)propanoate)

Guidance literature:: Multi-step reaction with 3 steps

1: trifluoroacetic acid / dichloromethane / 16 h / 20 °C

2: dmap; diisopropyl-carbodiimide / ethyl acetate / 96 h / 20 °C

3: hydrogen; palladium 10% on activated carbon / methanol / 45 °C / 7500.75 Torr

With dmap; palladium 10% on activated carbon; hydrogen; trifluoroacetic acid; diisopropyl-carbodiimide; In methanol; dichloromethane; ethyl acetate;

Reference yield:

: 1443300-56-8
tert-butyl 3-(2-(2-hydroxyethoxy)ethoxy)-2,2-dimethylpropanoate

: 1443300-35-3
2,5-bis(dimethylcarbamoyl)-1-(4-methoxyphenyl)-1-pyrrole-3,4-diyl bis(2,2-dimethyl-3-(2-(2-(phosphonooxy)ethoxy)ethoxy)propanoate)

Guidance literature:: Multi-step reaction with 4 steps

1.1: 5-methyl-1,2,3,4-tetrazole / tetrahydrofuran / 1.5 h / 20 °C

1.2: 16 h / 0 - 20 °C

2.1: trifluoroacetic acid / dichloromethane / 16 h / 20 °C

3.1: dmap; diisopropyl-carbodiimide / ethyl acetate / 96 h / 20 °C

4.1: hydrogen; palladium 10% on activated carbon / methanol / 45 °C / 7500.75 Torr

With 5-methyl-1,2,3,4-tetrazole; dmap; palladium 10% on activated carbon; hydrogen; trifluoroacetic acid; diisopropyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate;