3-(2-(2-((bis(benzyloxy)phosphoryl)oxy)ethoxy)ethoxy)-2,2-dimethylpropanoic acid

Base Information

Chemical Name:3-(2-(2-((bis(benzyloxy)phosphoryl)oxy)ethoxy)ethoxy)-2,2-dimethylpropanoic acid
CAS No.:1443300-58-0
Molecular Formula:C₂₃H₃₁O₈P
Molecular Weight:466.468
Hs Code.:

Synonyms:3-(2-(2-((bis(benzyloxy)phosphoryl)oxy)ethoxy)ethoxy)-2,2-dimethylpropanoic acid

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Chemical Property of 3-(2-(2-((bis(benzyloxy)phosphoryl)oxy)ethoxy)ethoxy)-2,2-dimethylpropanoic acid

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Technology Process of 3-(2-(2-((bis(benzyloxy)phosphoryl)oxy)ethoxy)ethoxy)-2,2-dimethylpropanoic acid

There total 3 articles about 3-(2-(2-((bis(benzyloxy)phosphoryl)oxy)ethoxy)ethoxy)-2,2-dimethylpropanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1443300-57-9
tert-butyl 3-(2-(2-((bis(benzyloxy)phosphoryl)oxy)ethoxy)ethoxy)-2,2-dimethylpropanoate

: 1443300-58-0
3-(2-(2-((bis(benzyloxy)phosphoryl)oxy)ethoxy)ethoxy)-2,2-dimethylpropanoic acid

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 16h;

Reference yield:

: 1443300-56-8
tert-butyl 3-(2-(2-hydroxyethoxy)ethoxy)-2,2-dimethylpropanoate

: 1443300-58-0
3-(2-(2-((bis(benzyloxy)phosphoryl)oxy)ethoxy)ethoxy)-2,2-dimethylpropanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: 5-methyl-1,2,3,4-tetrazole / tetrahydrofuran / 1.5 h / 20 °C

1.2: 16 h / 0 - 20 °C

2.1: trifluoroacetic acid / dichloromethane / 16 h / 20 °C

With 5-methyl-1,2,3,4-tetrazole; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;

Reference yield:

: 1443300-55-7
tert-butyl 3-(2-(2-(benzyloxy)ethoxy)ethoxy)-2,2-dimethylpropanoate

: 1443300-58-0
3-(2-(2-((bis(benzyloxy)phosphoryl)oxy)ethoxy)ethoxy)-2,2-dimethylpropanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen; palladium 10% on activated carbon / ethanol / 16 h / 3750.38 Torr

2.1: 5-methyl-1,2,3,4-tetrazole / tetrahydrofuran / 1.5 h / 20 °C

2.2: 16 h / 0 - 20 °C

3.1: trifluoroacetic acid / dichloromethane / 16 h / 20 °C

With 5-methyl-1,2,3,4-tetrazole; palladium 10% on activated carbon; hydrogen; trifluoroacetic acid; In tetrahydrofuran; ethanol; dichloromethane;