2,5-bis(dimethylcarbamoyl)-1-(4-methoxyphenyl)-1H-pyrrole-3,4-diyl bis(3-(2-(2-((bis(benzyloxy)phosphoryl)oxy)ethoxy)ethoxy)-2,2-dimethylpropanoate)

Base Information

Chemical Name:2,5-bis(dimethylcarbamoyl)-1-(4-methoxyphenyl)-1H-pyrrole-3,4-diyl bis(3-(2-(2-((bis(benzyloxy)phosphoryl)oxy)ethoxy)ethoxy)-2,2-dimethylpropanoate)
CAS No.:1443300-67-1
Molecular Formula:C₆₃H₇₉N₃O₁₉P₂
Molecular Weight:1244.28
Hs Code.:

2,5-bis(dimethylcarbamoyl)-1-(4-methoxyphenyl)-1H-pyrrole-3,4-diyl bis(3-(2-(2-((bis(benzyloxy)phosphoryl)oxy)ethoxy)ethoxy)-2,2-dimethylpropanoate)

Synonyms:2,5-bis(dimethylcarbamoyl)-1-(4-methoxyphenyl)-1H-pyrrole-3,4-diyl bis(3-(2-(2-((bis(benzyloxy)phosphoryl)oxy)ethoxy)ethoxy)-2,2-dimethylpropanoate)

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Chemical Property of 2,5-bis(dimethylcarbamoyl)-1-(4-methoxyphenyl)-1H-pyrrole-3,4-diyl bis(3-(2-(2-((bis(benzyloxy)phosphoryl)oxy)ethoxy)ethoxy)-2,2-dimethylpropanoate)

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Technology Process of 2,5-bis(dimethylcarbamoyl)-1-(4-methoxyphenyl)-1H-pyrrole-3,4-diyl bis(3-(2-(2-((bis(benzyloxy)phosphoryl)oxy)ethoxy)ethoxy)-2,2-dimethylpropanoate)

There total 4 articles about 2,5-bis(dimethylcarbamoyl)-1-(4-methoxyphenyl)-1H-pyrrole-3,4-diyl bis(3-(2-(2-((bis(benzyloxy)phosphoryl)oxy)ethoxy)ethoxy)-2,2-dimethylpropanoate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 1443052-72-9
3,4-dihydroxy-1-(4-methoxyphenyl)-N²,N²,N⁵,N⁵-tetramethyl-1H-pyrrole-2,5-dicarboxamide

: 1443300-58-0
3-(2-(2-((bis(benzyloxy)phosphoryl)oxy)ethoxy)ethoxy)-2,2-dimethylpropanoic acid

: 1443300-67-1
2,5-bis(dimethylcarbamoyl)-1-(4-methoxyphenyl)-1H-pyrrole-3,4-diyl bis(3-(2-(2-((bis(benzyloxy)phosphoryl)oxy)ethoxy)ethoxy)-2,2-dimethylpropanoate)

Guidance literature:: With dmap; diisopropyl-carbodiimide; In ethyl acetate; at 20 ℃; for 96h;

Reference yield:

: 1443300-56-8
tert-butyl 3-(2-(2-hydroxyethoxy)ethoxy)-2,2-dimethylpropanoate

: 1443300-67-1
2,5-bis(dimethylcarbamoyl)-1-(4-methoxyphenyl)-1H-pyrrole-3,4-diyl bis(3-(2-(2-((bis(benzyloxy)phosphoryl)oxy)ethoxy)ethoxy)-2,2-dimethylpropanoate)

Guidance literature:: Multi-step reaction with 3 steps

1.1: 5-methyl-1,2,3,4-tetrazole / tetrahydrofuran / 1.5 h / 20 °C

1.2: 16 h / 0 - 20 °C

2.1: trifluoroacetic acid / dichloromethane / 16 h / 20 °C

3.1: dmap; diisopropyl-carbodiimide / ethyl acetate / 96 h / 20 °C

With 5-methyl-1,2,3,4-tetrazole; dmap; trifluoroacetic acid; diisopropyl-carbodiimide; In tetrahydrofuran; dichloromethane; ethyl acetate;

Reference yield:

: 1443300-55-7
tert-butyl 3-(2-(2-(benzyloxy)ethoxy)ethoxy)-2,2-dimethylpropanoate

: 1443300-67-1
2,5-bis(dimethylcarbamoyl)-1-(4-methoxyphenyl)-1H-pyrrole-3,4-diyl bis(3-(2-(2-((bis(benzyloxy)phosphoryl)oxy)ethoxy)ethoxy)-2,2-dimethylpropanoate)

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogen; palladium 10% on activated carbon / ethanol / 16 h / 3750.38 Torr

2.1: 5-methyl-1,2,3,4-tetrazole / tetrahydrofuran / 1.5 h / 20 °C

2.2: 16 h / 0 - 20 °C

3.1: trifluoroacetic acid / dichloromethane / 16 h / 20 °C

4.1: dmap; diisopropyl-carbodiimide / ethyl acetate / 96 h / 20 °C

With 5-methyl-1,2,3,4-tetrazole; dmap; palladium 10% on activated carbon; hydrogen; trifluoroacetic acid; diisopropyl-carbodiimide; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate;