N-benzyl-1,1-diphenylmethanimine oxide

Base Information

• Chemical Name: N-benzyl-1,1-diphenylmethanimine oxide
• CAS No.: 3376-29-2
• Molecular Formula: C₂₀H₁₇NO
• Molecular Weight: 287.361
• Mol file: 3376-29-2.mol

Synonyms:N-benzyl-1,1-diphenylmethanimine oxide

Chemical Property of N-benzyl-1,1-diphenylmethanimine oxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-benzyl-1,1-diphenylmethanimine oxide

There total 9 articles about N-benzyl-1,1-diphenylmethanimine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

2-benzyl-3,3-diphenyl-1,2-oxaziridine → N-benzyl-1,1-diphenylmethanimine oxide (3376-29-2)

Guidance literature:

With 9-(2-mesityl)-10-methylacridinium perchlorate; In water; acetonitrile; at 20 ℃; for 24h; Inert atmosphere; Irradiation;

DOI:10.1021/acs.orglett.7b03369

Reference yield:

Benzophenone oxime (574-66-3) + benzyl bromide (100-39-0) → benzophenone (119-61-9) + methanone-diphenyl-O-(phenylmethyl)oxime (3362-43-4) + N-benzyl-1,1-diphenylmethanimine oxide (3376-29-2)

Guidance literature:

Multistep reaction; (i) EtONa, EtOH, (ii) /BRN= 385801/;

DOI:10.1021/ja00866a027

Reference yield:

benzylamine (100-46-9) → N-benzyl-1,1-diphenylmethanimine oxide (3376-29-2)

Guidance literature:

Multi-step reaction with 3 steps

1: toluene / 24 h / Dean-Stark; Molecular sieve; Inert atmosphere; Reflux

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 °C / Inert atmosphere

3: 9-(2-mesityl)-10-methylacridinium perchlorate / acetonitrile; water / 24 h / 20 °C / Inert atmosphere; Irradiation

With 3-chloro-benzenecarboperoxoic acid; 9-(2-mesityl)-10-methylacridinium perchlorate; In dichloromethane; water; toluene; acetonitrile;

DOI:10.1021/acs.orglett.7b03369

upstream raw materials:

N-benzhydryl-N-benzyl-hydroxylamine

benzophenone oxime ; sodium salt

iodomethylbenzene

Benzophenone oxime

Downstream raw materials:

N-benzhydryl-N-benzyl-hydroxylamine

N-benzyl hydroxylalmine

benzophenone