N-[1-cyano-2-(2,4-dichlorophenoxy)-1-methylethyl]-4-(pentafluorothio)benzamide

Base Information

Chemical Name:N-[1-cyano-2-(2,4-dichlorophenoxy)-1-methylethyl]-4-(pentafluorothio)benzamide
CAS No.:1046446-46-1
Molecular Formula:C₁₇H₁₃Cl₂F₅N₂O₂S
Molecular Weight:475.266
Hs Code.:

Synonyms:N-[1-cyano-2-(2,4-dichlorophenoxy)-1-methylethyl]-4-(pentafluorothio)benzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[1-cyano-2-(2,4-dichlorophenoxy)-1-methylethyl]-4-(pentafluorothio)benzamide

Chemical Property:

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Technology Process of N-[1-cyano-2-(2,4-dichlorophenoxy)-1-methylethyl]-4-(pentafluorothio)benzamide

There total 6 articles about N-[1-cyano-2-(2,4-dichlorophenoxy)-1-methylethyl]-4-(pentafluorothio)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1046820-87-4,1046447-02-2,1046820-88-5
N-(1-cyano-2-hydroxy-1-methylethyl)-4-(pentafluorothio)benzamide

: 1435-48-9
1,3-dichloro-4-fluorobenzene

: 1046446-46-1
N-[1-cyano-2-(2,4-dichlorophenoxy)-1-methylethyl]-4-(pentafluorothio)benzamide

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; dimethyl sulfoxide; at 20 ℃; for 18h;

Reference yield:

: 1046446-99-4
pentafluoro(4-vinylphenyl)-λ⁶-sulfane

: 1046446-46-1
N-[1-cyano-2-(2,4-dichlorophenoxy)-1-methylethyl]-4-(pentafluorothio)benzamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium periodate / ruthenium trichloride / tetrachloromethane; water; acetonitrile / 1 h / 20 °C

1.2: pH 1

2.1: thionyl chloride / 4 h / 65 °C

3.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 h / -10 °C

4.1: potassium tert-butylate / tetrahydrofuran; dimethyl sulfoxide / 18 h / 20 °C

With sodium periodate; thionyl chloride; potassium tert-butylate; N-ethyl-N,N-diisopropylamine; ruthenium trichloride; In tetrahydrofuran; tetrachloromethane; water; dimethyl sulfoxide; acetonitrile;

Reference yield:

: 2993-24-0
4-(pentafluorosulfanyl)aniline

: 1046446-46-1
N-[1-cyano-2-(2,4-dichlorophenoxy)-1-methylethyl]-4-(pentafluorothio)benzamide

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogenchloride; sodium nitrite / water / 0.03 h / 0 °C

1.2: 60 h / 0 - 20 °C

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 1.5 h / 100 °C

3.1: sodium periodate / ruthenium trichloride / tetrachloromethane; water; acetonitrile / 1 h / 20 °C

3.2: pH 1

4.1: thionyl chloride / 4 h / 65 °C

5.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 h / -10 °C

6.1: potassium tert-butylate / tetrahydrofuran; dimethyl sulfoxide / 18 h / 20 °C

With hydrogenchloride; sodium periodate; thionyl chloride; potassium tert-butylate; N-ethyl-N,N-diisopropylamine; sodium nitrite; ruthenium trichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; tetrachloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;