2-N-(4,4'-dimethoxytrityl)-2',3'-O-methoxymethyleneguanosine-5' S,S-diphenyl dithiophosphate

Base Information

Chemical Name:2-N-(4,4'-dimethoxytrityl)-2',3'-O-methoxymethyleneguanosine-5' S,S-diphenyl dithiophosphate
CAS No.:98151-67-8
Molecular Formula:C₄₅H₄₂N₅O₉PS₂
Molecular Weight:891.962
Hs Code.:

Synonyms:2-N-(4,4'-dimethoxytrityl)-2',3'-O-methoxymethyleneguanosine-5' S,S-diphenyl dithiophosphate

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Chemical Property of 2-N-(4,4'-dimethoxytrityl)-2',3'-O-methoxymethyleneguanosine-5' S,S-diphenyl dithiophosphate

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Technology Process of 2-N-(4,4'-dimethoxytrityl)-2',3'-O-methoxymethyleneguanosine-5' S,S-diphenyl dithiophosphate

There total 4 articles about 2-N-(4,4'-dimethoxytrityl)-2',3'-O-methoxymethyleneguanosine-5' S,S-diphenyl dithiophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 67941-87-1
cyclohexylammonium S,S-diphenyl phosphorodithioate

: 98151-72-5
2-N-(4,4'-dimethoxytrityl)-2',3'-di-O-methoxymethyleneguanosine

: 98151-67-8
2-N-(4,4'-dimethoxytrityl)-2',3'-O-methoxymethyleneguanosine-5' S,S-diphenyl dithiophosphate

Guidance literature:: With 2,3-dimercapto-succinic acid; In pyridine; for 2h;
DOI:10.1039/P19850000997

Reference yield:

: 98151-64-5
5'-O-acetyl-2-N-(4,4'-dimethoxytrityl)guanosine

: 98151-67-8
2-N-(4,4'-dimethoxytrityl)-2',3'-O-methoxymethyleneguanosine-5' S,S-diphenyl dithiophosphate

Guidance literature:: Multi-step reaction with 3 steps

1: TpSA*H₂O, molecular sieves 3A / dioxane / 0.02 h

2: butylamine, MeOH / 3 h

3: 81 percent / DMS / pyridine / 2 h

With methanol; 2,3-dimercapto-succinic acid; 3 A molecular sieve; TpSA*H₂O; N-butylamine; In 1,4-dioxane; pyridine;
DOI:10.1039/P19850000997

Reference yield:

: 98151-65-6
Acetic acid (3aR,4R,6R,6aR)-6-(2-{[bis-(4-methoxy-phenyl)-phenyl-methyl]-amino}-6-oxo-1,6-dihydro-purin-9-yl)-2-methoxy-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

: 98151-67-8
2-N-(4,4'-dimethoxytrityl)-2',3'-O-methoxymethyleneguanosine-5' S,S-diphenyl dithiophosphate

Guidance literature:: Multi-step reaction with 2 steps

1: butylamine, MeOH / 3 h

2: 81 percent / DMS / pyridine / 2 h

With methanol; 2,3-dimercapto-succinic acid; N-butylamine; In pyridine;
DOI:10.1039/P19850000997