p-Nitrobenzaldehyde O-methyloxime

Base Information

Chemical Name:p-Nitrobenzaldehyde O-methyloxime
CAS No.:33499-32-0
Molecular Formula:C8H8N2O3
Molecular Weight:180.163
Hs Code.:
NSC Number:167074
Mol file:33499-32-0.mol

Synonyms:p-Nitrobenzaldehyde O-methyloxime;O-Methyl-p-nitrobenzaldoxime;Benzaldehyde, p-nitro-, O-methyloxime;Benzaldehyde, 4-nitro-, O-methyloxime;33499-32-0;SCHEMBL9841029;ONZBYRQWJOKYPR-RMKNXTFCSA-N;4-Nitrobenzaldehyde o-methyloxime #;NSC167074;NSC-167074

Suppliers and Price of p-Nitrobenzaldehyde O-methyloxime

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of p-Nitrobenzaldehyde O-methyloxime

Chemical Property:

Vapor Pressure:0.004mmHg at 25°C
Boiling Point:287.3°Cat760mmHg
Flash Point:127.6°C
PSA：67.41000
Density:1.21g/cm³
LogP:2.09830
XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:180.05349212
Heavy Atom Count:13
Complexity:192

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CON=CC1=CC=C(C=C1)[N+](=O)[O-]
Isomeric SMILES:CO/N=C/C1=CC=C(C=C1)[N+](=O)[O-]

Technology Process of p-Nitrobenzaldehyde O-methyloxime

There total 4 articles about p-Nitrobenzaldehyde O-methyloxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 619-73-8
4-nitrobenzyl chloride

: 593-56-6
N-methoxylamine hydrochloride

: 33499-32-0
(E/Z)-4-nitrobenzaldehyde O-methyl oxime

Guidance literature:: With manganese(IV) oxide; 4 A molecular sieve; In dichloromethane; for 22h; Heating;
DOI:10.1055/s-2002-32949

Reference yield:

: 593-56-6
N-methoxylamine hydrochloride

: 555-16-8
4-nitrobenzaldehdye

: 33499-32-0
(E/Z)-4-nitrobenzaldehyde O-methyl oxime

Guidance literature:: With pyridine; In ethanol;
DOI:10.1021/jo01258a062

Reference yield:

: 74-88-4
methyl iodide

: 1129-37-9,174848-02-3,20707-69-1
4-nitrobenzaldehyde oxime

: 33499-32-0
(E/Z)-4-nitrobenzaldehyde O-methyl oxime

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) DMF, room temp., 10 min, 2.) DMF, 30 min;
DOI:10.1021/jo00166a035