{N-[4-(α-D-mannopyranosyloxy)phenyl]-N’-[(2‘-tert-butyloxycarbonylamido)ethyl]}squaric acid diamide

Base Information

Chemical Name:{N-[4-(α-D-mannopyranosyloxy)phenyl]-N’-[(2‘-tert-butyloxycarbonylamido)ethyl]}squaric acid diamide
CAS No.:1417341-50-4
Molecular Formula:C₂₃H₃₁N₃O₁₀
Molecular Weight:509.513
Hs Code.:

Synonyms:{N-[4-(α-D-mannopyranosyloxy)phenyl]-N’-[(2‘-tert-butyloxycarbonylamido)ethyl]}squaric acid diamide

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Chemical Property of {N-[4-(α-D-mannopyranosyloxy)phenyl]-N’-[(2‘-tert-butyloxycarbonylamido)ethyl]}squaric acid diamide

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Technology Process of {N-[4-(α-D-mannopyranosyloxy)phenyl]-N’-[(2‘-tert-butyloxycarbonylamido)ethyl]}squaric acid diamide

There total 4 articles about {N-[4-(α-D-mannopyranosyloxy)phenyl]-N’-[(2‘-tert-butyloxycarbonylamido)ethyl]}squaric acid diamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 57260-73-8
N-BOC-1,2-diaminoethane

: N-{[4-(α-D-mannopyranosyloxy)phenyl]amido}squaric acidmethyl ester

: 1417341-50-4
{N-[4-(α-D-mannopyranosyloxy)phenyl]-N’-[(2‘-tert-butyloxycarbonylamido)ethyl]}squaric acid diamide

Guidance literature:: With triethylamine; In methanol; at 20 ℃; for 15h;
DOI:10.3762/bjoc.14.163

Reference yield: 92.0%

: 916849-16-6
3-ethoxy-4-[[4-(α-D-mannopyranosyloxy)phenyl]amino]-3-cyclobutene-1,2-dione

: 57260-73-8
N-BOC-1,2-diaminoethane

: 1417341-50-4
{N-[4-(α-D-mannopyranosyloxy)phenyl]-N’-[(2‘-tert-butyloxycarbonylamido)ethyl]}squaric acid diamide

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 18h;
DOI:10.1002/cbic.201200365

Reference yield:

: 10357-27-4
4-nitrophenyl-α-D-mannopyranoside

: 1417341-50-4
{N-[4-(α-D-mannopyranosyloxy)phenyl]-N’-[(2‘-tert-butyloxycarbonylamido)ethyl]}squaric acid diamide

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen; palladium on activated charcoal / methanol / 6 h / 20 °C

2: methanol / 16 h / 20 °C

3: triethylamine / methanol / 15 h / 20 °C

With palladium on activated charcoal; hydrogen; triethylamine; In methanol;
DOI:10.3762/bjoc.14.163