p-[((2-aminoethylamino)-2,3-dioxocyclobut-1-enyl)amino]phenyl α-D-mannopyranoside

Base Information

Chemical Name:p-[((2-aminoethylamino)-2,3-dioxocyclobut-1-enyl)amino]phenyl α-D-mannopyranoside
CAS No.:1417341-51-5
Molecular Formula:C₁₈H₂₃N₃O₈
Molecular Weight:409.396
Hs Code.:

Synonyms:p-[((2-aminoethylamino)-2,3-dioxocyclobut-1-enyl)amino]phenyl α-D-mannopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-[((2-aminoethylamino)-2,3-dioxocyclobut-1-enyl)amino]phenyl α-D-mannopyranoside

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Technology Process of p-[((2-aminoethylamino)-2,3-dioxocyclobut-1-enyl)amino]phenyl α-D-mannopyranoside

There total 3 articles about p-[((2-aminoethylamino)-2,3-dioxocyclobut-1-enyl)amino]phenyl α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1417341-50-4
{N-[4-(α-D-mannopyranosyloxy)phenyl]-N’-[(2‘-tert-butyloxycarbonylamido)ethyl]}squaric acid diamide

: 1417341-51-5
p-[((2-aminoethylamino)-2,3-dioxocyclobut-1-enyl)amino]phenyl α-D-mannopyranoside

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1002/cbic.201200365

Reference yield:

: 10357-27-4
4-nitrophenyl-α-D-mannopyranoside

: 1417341-51-5
p-[((2-aminoethylamino)-2,3-dioxocyclobut-1-enyl)amino]phenyl α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen; palladium on activated charcoal / methanol / 6 h / 20 °C

2: methanol / 16 h / 20 °C

3: triethylamine / methanol / 15 h / 20 °C

4: trifluoroacetic acid / water / 3 h / 20 °C

With palladium on activated charcoal; hydrogen; triethylamine; trifluoroacetic acid; In methanol; water;
DOI:10.3762/bjoc.14.163

Reference yield:

: 34213-86-0
p-aminophenyl-α-D-mannopyranoside

: 1417341-51-5
p-[((2-aminoethylamino)-2,3-dioxocyclobut-1-enyl)amino]phenyl α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 16 h / 20 °C

2: triethylamine / methanol / 15 h / 20 °C

3: trifluoroacetic acid / water / 3 h / 20 °C

With triethylamine; trifluoroacetic acid; In methanol; water;
DOI:10.3762/bjoc.14.163