2-i-PrC₆H₄P(SiMe₃)2

Base Information

Chemical Name:2-i-PrC₆H₄P(SiMe₃)2
CAS No.:1237893-84-3
Molecular Formula:C₁₅H₂₉PSi₂
Molecular Weight:296.54
Hs Code.:

2-i-PrC<sub>6</sub>H<sub>4</sub>P(SiMe<sub>3</sub>)2

Synonyms:2-i-PrC₆H₄P(SiMe₃)2

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Chemical Property of 2-i-PrC₆H₄P(SiMe₃)2

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Technology Process of 2-i-PrC₆H₄P(SiMe₃)2

There total 12 articles about 2-i-PrC₆H₄P(SiMe₃)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 75-77-4
chloro-trimethyl-silane

: 915199-68-7
2-i-PrC₆H₄PH₂

: 1237893-84-3
2-i-PrC₆H₄P(SiMe₃)2

Guidance literature:: 2-i-PrC₆H₄PH₂; With methyllithium; In tetrahydrofuran; diethyl ether; at -78 - 20 ℃; Inert atmosphere;

With chloro-trimethyl-silane; In tetrahydrofuran; diethyl ether; at -78 ℃; Inert atmosphere;

chloro-trimethyl-silane; Further stages;
DOI:10.1002/hc.20619

Reference yield:

: 915199-68-7
2-i-PrC₆H₄PH₂

: 2-i-PrC₆H₄PH(SiMe₃)

: 1237893-84-3
2-i-PrC₆H₄P(SiMe₃)2

Guidance literature:: 2-i-PrC₆H₄PH₂; With methyllithium; In tetrahydrofuran; diethyl ether; at -78 - 20 ℃; Inert atmosphere;

With chloro-trimethyl-silane; In tetrahydrofuran; diethyl ether; at -78 ℃; Inert atmosphere;
DOI:10.1002/hc.20619

Reference yield:

: 643-28-7
2-isopropylaniline

: 1237893-84-3
2-i-PrC₆H₄P(SiMe₃)2

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogen bromide; sodium nitrite / Inert atmosphere

1.2: Inert atmosphere

2.1: magnesium / tetrahydrofuran / 20 °C / Inert atmosphere; Reflux

2.2: 20 °C / Inert atmosphere

3.1: hydrogenchloride / dichloromethane / Inert atmosphere

4.1: lithium aluminium tetrahydride / diethyl ether / -78 - 20 °C / Inert atmosphere

5.1: methyllithium / tetrahydrofuran; diethyl ether / -78 - 20 °C / Inert atmosphere

5.2: -78 °C / Inert atmosphere

With hydrogenchloride; lithium aluminium tetrahydride; hydrogen bromide; methyllithium; magnesium; sodium nitrite; In tetrahydrofuran; diethyl ether; dichloromethane; 1.1: Sandmeyer reaction / 1.2: Sandmeyer reaction;
DOI:10.1002/hc.20619