N-benzoyl-2'-O-[N₂,N₆-bis(trifluoroacetyl)lysyl]aminohexyl-5'-O-(4,4'-dimethoxytrityl)adenosine

Base Information

• Chemical Name: N-benzoyl-2'-O-[N₂,N₆-bis(trifluoroacetyl)lysyl]aminohexyl-5'-O-(4,4'-dimethoxytrityl)adenosine
• CAS No.: 1242674-91-4
• Molecular Formula: C₅₄H₅₈F₆N₈O₁₀
• Molecular Weight: 1093.09

Synonyms:N-benzoyl-2'-O-[N₂,N₆-bis(trifluoroacetyl)lysyl]aminohexyl-5'-O-(4,4'-dimethoxytrityl)adenosine

Chemical Property of N-benzoyl-2'-O-[N₂,N₆-bis(trifluoroacetyl)lysyl]aminohexyl-5'-O-(4,4'-dimethoxytrityl)adenosine

Chemical Property:

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Technology Process of N-benzoyl-2'-O-[N₂,N₆-bis(trifluoroacetyl)lysyl]aminohexyl-5'-O-(4,4'-dimethoxytrityl)adenosine

There total 1 articles about N-benzoyl-2'-O-[N₂,N₆-bis(trifluoroacetyl)lysyl]aminohexyl-5'-O-(4,4'-dimethoxytrityl)adenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

2'-O-[N2,N6-bis(trifluoroacetyl)lysyl]aminohexyl-5'-O-(4,4'-dimethoxytrityl)adenosine (1242674-89-0) + benzoyl chloride (98-88-4) → N-benzoyl-2'-O-[N2,N6-bis(trifluoroacetyl)lysyl]aminohexyl-5'-O-(4,4'-dimethoxytrityl)adenosine (1242674-91-4)

Guidance literature:

2'-O-[N₂,N₆-bis(trifluoroacetyl)lysyl]aminohexyl-5'-O-(4,4'-dimethoxytrityl)adenosine; With pyridine; chloro-trimethyl-silane; In dichloromethane; at 20 ℃; Inert atmosphere;

benzoyl chloride; In dichloromethane; at 20 ℃; for 16h; Inert atmosphere;

DOI:10.1007/s00706-010-0318-0

Reference yield: 59.0%

N-benzoyl-2'-O-[N2,N6-bis(trifluoroacetyl)lysyl]aminohexyl-5'-O-(4,4'-dimethoxytrityl)adenosine (1242674-91-4) + N,N,N',N'-tetraisopropyl 2-cyanoethylphosphorodiamidite (102691-36-1) → N-benzoyl-2'-O-[N2,N6-bis(trifluoroacetyl)lysyl]aminohexyl-5'-O-(4,4'-dimethoxytrityl)adenosine 3'-O-[O-(2-cyanoethyl)-N,N-diisopropylphosphoramidite] (1242674-93-6)

Guidance literature:

With 1H-tetrazole; In dichloromethane; at 20 ℃; for 16h; Inert atmosphere;

DOI:10.1007/s00706-010-0318-0

upstream raw materials:

2'-O-[N₂,N₆-bis(trifluoroacetyl)lysyl]aminohexyl-5'-O-(4,4'-dimethoxytrityl)adenosine

benzoyl chloride

Downstream raw materials:

N-benzoyl-2'-O-[N₂,N₆-bis(trifluoroacetyl)lysyl]aminohexyl-5'-O-(4,4'-dimethoxytrityl)adenosine 3'-O-[O-(2-cyanoethyl)-N,N-diisopropylphosphoramidite]

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