6,6'-((1,4-phenylenebis(azanylylidene))bis(methanylylidene))bis(2-methoxyphenol)

Base Information

Chemical Name:6,6'-((1,4-phenylenebis(azanylylidene))bis(methanylylidene))bis(2-methoxyphenol)
CAS No.:19264-44-9
Molecular Formula:C₂₂H₂₀N₂O₄
Molecular Weight:376.412
Hs Code.:

Synonyms:6,6'-((1,4-phenylenebis(azanylylidene))bis(methanylylidene))bis(2-methoxyphenol)

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Chemical Property of 6,6'-((1,4-phenylenebis(azanylylidene))bis(methanylylidene))bis(2-methoxyphenol)

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Technology Process of 6,6'-((1,4-phenylenebis(azanylylidene))bis(methanylylidene))bis(2-methoxyphenol)

There total 1 articles about 6,6'-((1,4-phenylenebis(azanylylidene))bis(methanylylidene))bis(2-methoxyphenol) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 148-53-8
3-methoxy-2-hydroxybenzaldehyde

: 106-50-3
1,4-phenylenediamine

: 19264-44-9
6,6'-((1,4-phenylenebis(azanylylidene))bis(methanylylidene))bis(2-methoxyphenol)

Guidance literature:: In ethanol; for 5h; Reflux;
DOI:10.1039/c4ra10692j

Reference yield: 42.0%

: 879089-16-4,155065-88-6
[Cu₂(OAc)4(H₂O)2]

: 19264-44-9
6,6'-((1,4-phenylenebis(azanylylidene))bis(methanylylidene))bis(2-methoxyphenol)

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: [(copper(II))4(N,N'-bis-(3-methoxy-salycilidene)benzene-1,4-diamine)4] dimethylformamide disolvate

Guidance literature:: In N,N-dimethyl-formamide; soln. of Cu(OAc)2*2H2O (0.2 mmol) and H2bmsbd (0.2 mmol) refluxed, cooled to room temp.; filtered, crystd. by slow diffusing diethyl ether vapour; elem. anal.;
DOI:10.1016/j.ica.2009.08.003

Reference yield:

: 19264-44-9
6,6'-((1,4-phenylenebis(azanylylidene))bis(methanylylidene))bis(2-methoxyphenol)

: 557-34-6
zinc diacetate

: 2Zn⁽²⁺⁾*2C₆H₄(NCHC₆H₃(O)OCH₃)2^(2-)*2H₂O=[Zn(C₆H₄(NCHC₆H₃(O)OCH₃)2)(H₂O)]2

Guidance literature:: In methanol; refluxing equimolar amts. for 3 h; pptn. on cooling to room temp., filtration, drying (vac.); elem. anal.;
DOI:10.1016/S0022-328X(98)00417-3