1,6,7,12-tetrakis(4-n-butyloxyphenoxy)perylene-3,4,9,10-tetracarboxylic acid dianhydride

Base Information

• Chemical Name: 1,6,7,12-tetrakis(4-n-butyloxyphenoxy)perylene-3,4,9,10-tetracarboxylic acid dianhydride
• CAS No.: 530086-49-8
• Molecular Formula: C₆₄H₅₆O₁₄
• Molecular Weight: 1049.14

Synonyms:1,6,7,12-tetrakis(4-n-butyloxyphenoxy)perylene-3,4,9,10-tetracarboxylic acid dianhydride

Chemical Property of 1,6,7,12-tetrakis(4-n-butyloxyphenoxy)perylene-3,4,9,10-tetracarboxylic acid dianhydride

Chemical Property:

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Technology Process of 1,6,7,12-tetrakis(4-n-butyloxyphenoxy)perylene-3,4,9,10-tetracarboxylic acid dianhydride

There total 5 articles about 1,6,7,12-tetrakis(4-n-butyloxyphenoxy)perylene-3,4,9,10-tetracarboxylic acid dianhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

N,N'-bis(n-butyl)-1,6,7,12-tetrakis(4-n-butyloxyphenoxy)perylene-3,4,9,10-tetracarboxylic acid diimide (875752-66-2) → 1,6,7,12-tetrakis(4-n-butyloxyphenoxy)perylene-3,4,9,10-tetracarboxylic acid dianhydride (530086-49-8)

Guidance literature:

With potassium hydroxide; In propan-1-ol; at 80 ℃; for 24h;

DOI:10.1039/b513847g

Reference yield: 80.0%

N,N'-bis-n-propyl-1,6,7,12-tetrakis(4-n-butyloxyphenoxy)perylene-3,4,9,10-tetracarboxdiimide (1234347-63-7) → 1,6,7,12-tetrakis(4-n-butyloxyphenoxy)perylene-3,4,9,10-tetracarboxylic acid dianhydride (530086-49-8)

Guidance literature:

With potassium hydroxide; In water; isopropyl alcohol; for 24h; Inert atmosphere; Reflux;

DOI:10.1080/15421406.2010.497101

Reference yield:

perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride (128-69-8) → 1,6,7,12-tetrakis(4-n-butyloxyphenoxy)perylene-3,4,9,10-tetracarboxylic acid dianhydride (530086-49-8)

Guidance literature:

Multi-step reaction with 4 steps

1.1: propan-1-ol; water / 12 h / 65 °C / Inert atmosphere

2.1: sulfuryl dichloride; iodobenzene; iodine / nitrobenzene / 14 h / 80 °C / Inert atmosphere

2.2: 6 h / Inert atmosphere

3.1: potassium carbonate / 1-methyl-pyrrolidin-2-one / 6 h / 160 °C / Inert atmosphere

4.1: potassium hydroxide / water; isopropyl alcohol / 24 h / Inert atmosphere; Reflux

With sulfuryl dichloride; iodobenzene; iodine; potassium carbonate; potassium hydroxide; In 1-methyl-pyrrolidin-2-one; propan-1-ol; water; nitrobenzene; isopropyl alcohol;

DOI:10.1080/15421406.2010.497101

upstream raw materials:

N,N'-bis(n-butyl)-1,6,7,12-tetrakis(4-n-butyloxyphenoxy)perylene-3,4,9,10-tetracarboxylic acid diimide

N,N'-bis-n-propyl-1,6,7,12-tetrakis(4-n-butyloxyphenoxy)perylene-3,4,9,10-tetracarboxdiimide

perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

N,N’-bis(propyl)perylene-3,4,9,10-bis(dicarboximide)

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