N,N'-bis-n-propyl-1,6,7,12-tetrakis(4-n-butyloxyphenoxy)perylene-3,4,9,10-tetracarboxdiimide

Base Information

Chemical Name:N,N'-bis-n-propyl-1,6,7,12-tetrakis(4-n-butyloxyphenoxy)perylene-3,4,9,10-tetracarboxdiimide
CAS No.:1234347-63-7
Molecular Formula:C₇₀H₇₀N₂O₁₂
Molecular Weight:1131.33
Hs Code.:

Synonyms:N,N'-bis-n-propyl-1,6,7,12-tetrakis(4-n-butyloxyphenoxy)perylene-3,4,9,10-tetracarboxdiimide

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Chemical Property of N,N'-bis-n-propyl-1,6,7,12-tetrakis(4-n-butyloxyphenoxy)perylene-3,4,9,10-tetracarboxdiimide

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Technology Process of N,N'-bis-n-propyl-1,6,7,12-tetrakis(4-n-butyloxyphenoxy)perylene-3,4,9,10-tetracarboxdiimide

There total 3 articles about N,N'-bis-n-propyl-1,6,7,12-tetrakis(4-n-butyloxyphenoxy)perylene-3,4,9,10-tetracarboxdiimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 122-94-1
4-n-butoxyphenol

: N,N'-bis-n-propyl-1,6,7,12-tetrachloroperylene-3,4,9,10-tetracarboxdiimide

: 1234347-63-7
N,N'-bis-n-propyl-1,6,7,12-tetrakis(4-n-butyloxyphenoxy)perylene-3,4,9,10-tetracarboxdiimide

Guidance literature:: With potassium carbonate; In 1-methyl-pyrrolidin-2-one; at 160 ℃; for 6h; Inert atmosphere;
DOI:10.1080/15421406.2010.497101

Reference yield:

: 59442-38-5
N,N’-bis(propyl)perylene-3,4,9,10-bis(dicarboximide)

: 1234347-63-7
N,N'-bis-n-propyl-1,6,7,12-tetrakis(4-n-butyloxyphenoxy)perylene-3,4,9,10-tetracarboxdiimide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfuryl dichloride; iodobenzene; iodine / nitrobenzene / 14 h / 80 °C / Inert atmosphere

1.2: 6 h / Inert atmosphere

2.1: potassium carbonate / 1-methyl-pyrrolidin-2-one / 6 h / 160 °C / Inert atmosphere

With sulfuryl dichloride; iodobenzene; iodine; potassium carbonate; In 1-methyl-pyrrolidin-2-one; nitrobenzene;
DOI:10.1080/15421406.2010.497101

Reference yield:

: 128-69-8
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

: 1234347-63-7
N,N'-bis-n-propyl-1,6,7,12-tetrakis(4-n-butyloxyphenoxy)perylene-3,4,9,10-tetracarboxdiimide

Guidance literature:: Multi-step reaction with 3 steps

1.1: propan-1-ol; water / 12 h / 65 °C / Inert atmosphere

2.1: sulfuryl dichloride; iodobenzene; iodine / nitrobenzene / 14 h / 80 °C / Inert atmosphere

2.2: 6 h / Inert atmosphere

3.1: potassium carbonate / 1-methyl-pyrrolidin-2-one / 6 h / 160 °C / Inert atmosphere

With sulfuryl dichloride; iodobenzene; iodine; potassium carbonate; In 1-methyl-pyrrolidin-2-one; propan-1-ol; water; nitrobenzene;
DOI:10.1080/15421406.2010.497101