1-benzyloxycarbonyl-6S-(4,4-ethylenedioxybutyl)-2R-formylmethyl-4R-methylpiperidine

Base Information

Chemical Name:1-benzyloxycarbonyl-6S-(4,4-ethylenedioxybutyl)-2R-formylmethyl-4R-methylpiperidine
CAS No.:1436412-05-3
Molecular Formula:C₂₂H₃₁NO₅
Molecular Weight:389.492
Hs Code.:

Synonyms:1-benzyloxycarbonyl-6S-(4,4-ethylenedioxybutyl)-2R-formylmethyl-4R-methylpiperidine

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Chemical Property of 1-benzyloxycarbonyl-6S-(4,4-ethylenedioxybutyl)-2R-formylmethyl-4R-methylpiperidine

Chemical Property:

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Technology Process of 1-benzyloxycarbonyl-6S-(4,4-ethylenedioxybutyl)-2R-formylmethyl-4R-methylpiperidine

There total 4 articles about 1-benzyloxycarbonyl-6S-(4,4-ethylenedioxybutyl)-2R-formylmethyl-4R-methylpiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: C₃₂H₅₄BNO₄

: 1436412-05-3
1-benzyloxycarbonyl-6S-(4,4-ethylenedioxybutyl)-2R-formylmethyl-4R-methylpiperidine

Guidance literature:: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dimethyl sulfoxide; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ol4010917

Reference yield:

: C₂₆H₃₉NO₃

: 1436412-05-3
1-benzyloxycarbonyl-6S-(4,4-ethylenedioxybutyl)-2R-formylmethyl-4R-methylpiperidine

Guidance literature:: Multi-step reaction with 4 steps

1: lead(IV) tetraacetate / chloroform / 1 h / -50 °C / Inert atmosphere

2: potassium carbonate / tetrahydrofuran; water / 1 h / 0 °C / Inert atmosphere

3: tetrahydrofuran / 13 h / 20 °C / Inert atmosphere

4: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 3 h / 20 °C / Inert atmosphere

With lead(IV) tetraacetate; potassium carbonate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; chloroform; water; dimethyl sulfoxide;
DOI:10.1021/ol4010917

Reference yield:

: 1436412-02-0
6S-(4,4-ethylenedioxybutyl)-4R-methyl-2R-vinyl-piperidine

: 1436412-05-3
1-benzyloxycarbonyl-6S-(4,4-ethylenedioxybutyl)-2R-formylmethyl-4R-methylpiperidine

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / tetrahydrofuran; water / 1 h / 0 °C / Inert atmosphere

2: tetrahydrofuran / 13 h / 20 °C / Inert atmosphere

3: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 3 h / 20 °C / Inert atmosphere

With potassium carbonate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; water; dimethyl sulfoxide;
DOI:10.1021/ol4010917