1-benzyloxycarbonyl-6S-(4,4-ethylenedioxybutyl)-4R-methyl-2R-(2-oxo-propyl)piperidine

Base Information

Chemical Name:1-benzyloxycarbonyl-6S-(4,4-ethylenedioxybutyl)-4R-methyl-2R-(2-oxo-propyl)piperidine
CAS No.:1436412-07-5
Molecular Formula:C₂₃H₃₃NO₅
Molecular Weight:403.519
Hs Code.:

Synonyms:1-benzyloxycarbonyl-6S-(4,4-ethylenedioxybutyl)-4R-methyl-2R-(2-oxo-propyl)piperidine

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Chemical Property of 1-benzyloxycarbonyl-6S-(4,4-ethylenedioxybutyl)-4R-methyl-2R-(2-oxo-propyl)piperidine

Chemical Property:

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Technology Process of 1-benzyloxycarbonyl-6S-(4,4-ethylenedioxybutyl)-4R-methyl-2R-(2-oxo-propyl)piperidine

There total 6 articles about 1-benzyloxycarbonyl-6S-(4,4-ethylenedioxybutyl)-4R-methyl-2R-(2-oxo-propyl)piperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1436412-06-4
C₂₃H₃₅NO₅

: 1436412-07-5
1-benzyloxycarbonyl-6S-(4,4-ethylenedioxybutyl)-4R-methyl-2R-(2-oxo-propyl)piperidine

Guidance literature:: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dimethyl sulfoxide; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1021/ol4010917

Reference yield:

: C₂₆H₃₉NO₃

: 1436412-07-5
1-benzyloxycarbonyl-6S-(4,4-ethylenedioxybutyl)-4R-methyl-2R-(2-oxo-propyl)piperidine

Guidance literature:: Multi-step reaction with 6 steps

1: lead(IV) tetraacetate / chloroform / 1 h / -50 °C / Inert atmosphere

2: potassium carbonate / tetrahydrofuran; water / 1 h / 0 °C / Inert atmosphere

3: tetrahydrofuran / 13 h / 20 °C / Inert atmosphere

4: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 3 h / 20 °C / Inert atmosphere

5: tetrahydrofuran / 1 h / -10 °C / Inert atmosphere

6: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 4 h / 20 °C / Inert atmosphere

With lead(IV) tetraacetate; potassium carbonate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; chloroform; water; dimethyl sulfoxide;
DOI:10.1021/ol4010917

Reference yield:

: 1436412-02-0
6S-(4,4-ethylenedioxybutyl)-4R-methyl-2R-vinyl-piperidine

: 1436412-07-5
1-benzyloxycarbonyl-6S-(4,4-ethylenedioxybutyl)-4R-methyl-2R-(2-oxo-propyl)piperidine

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / tetrahydrofuran; water / 1 h / 0 °C / Inert atmosphere

2: tetrahydrofuran / 13 h / 20 °C / Inert atmosphere

3: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 3 h / 20 °C / Inert atmosphere

4: tetrahydrofuran / 1 h / -10 °C / Inert atmosphere

5: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 4 h / 20 °C / Inert atmosphere

With potassium carbonate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; water; dimethyl sulfoxide;
DOI:10.1021/ol4010917