dimethyl (((4-methylphenyl)sulfonamido)(4-nitrophenyl)methyl)phosphonate

Base Information

Chemical Name:dimethyl (((4-methylphenyl)sulfonamido)(4-nitrophenyl)methyl)phosphonate
CAS No.:1154063-22-5
Molecular Formula:C₁₆H₁₉N₂O₇PS
Molecular Weight:414.376
Hs Code.:

Synonyms:dimethyl (((4-methylphenyl)sulfonamido)(4-nitrophenyl)methyl)phosphonate

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Chemical Property of dimethyl (((4-methylphenyl)sulfonamido)(4-nitrophenyl)methyl)phosphonate

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Technology Process of dimethyl (((4-methylphenyl)sulfonamido)(4-nitrophenyl)methyl)phosphonate

There total 5 articles about dimethyl (((4-methylphenyl)sulfonamido)(4-nitrophenyl)methyl)phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 13707-46-5
N-tosyl-4-nitrobenzaldimine

: 868-85-9
Dimethyl phosphite

: 1154063-22-5
dimethyl (((4-methylphenyl)sulfonamido)(4-nitrophenyl)methyl)phosphonate

Guidance literature:: With 1,3-bis-(2,6-diisopropylphenyl)-imidazol-2-ylidene; In tetrahydrofuran; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1055/s-0031-1289690

Reference yield: 98.0%

: 36198-87-5
dimethyl trimethylsilyl phosphite

: 13707-46-5
N-tosyl-4-nitrobenzaldimine

: 1154063-22-5
dimethyl (((4-methylphenyl)sulfonamido)(4-nitrophenyl)methyl)phosphonate

Guidance literature:: dimethyl trimethylsilyl phosphite; N-tosyl-4-nitrobenzaldimine; In tetrahydrofuran; at 0 - 20 ℃; for 4h; Inert atmosphere;

With water; In tetrahydrofuran; for 0.5h; Inert atmosphere;
DOI:10.1002/cjoc.201200119