4-[3-(4-methanesulfonyl-phenyl)-[1,2,4]oxadiazol-5-ylmethyl]-piperidine hydrochloride

Base Information

• Chemical Name: 4-[3-(4-methanesulfonyl-phenyl)-[1,2,4]oxadiazol-5-ylmethyl]-piperidine hydrochloride
• CAS No.: 1103310-89-9
• Molecular Formula: C₁₅H₁₉N₃O₃S*ClH
• Molecular Weight: 357.861

Synonyms:4-[3-(4-methanesulfonyl-phenyl)-[1,2,4]oxadiazol-5-ylmethyl]-piperidine hydrochloride

Chemical Property of 4-[3-(4-methanesulfonyl-phenyl)-[1,2,4]oxadiazol-5-ylmethyl]-piperidine hydrochloride

Chemical Property:

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Technology Process of 4-[3-(4-methanesulfonyl-phenyl)-[1,2,4]oxadiazol-5-ylmethyl]-piperidine hydrochloride

There total 1 articles about 4-[3-(4-methanesulfonyl-phenyl)-[1,2,4]oxadiazol-5-ylmethyl]-piperidine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

4-[3-(4-methanesulfonyl-phenyl)-[1,2,4]oxadiazol-5-ylmethyl]-piperidine-1-carboxylic acid tert-butyl ester (1103310-87-7) → 4-[3-(4-methanesulfonyl-phenyl)-[1,2,4]oxadiazol-5-ylmethyl]-piperidine hydrochloride (1103310-89-9)

Guidance literature:

With hydrogenchloride; ethanol; In 1,4-dioxane; at 40 ℃; for 2.5h;

Reference yield:

4-[3-(4-methanesulfonyl-phenyl)-[1,2,4]oxadiazol-5-ylmethyl]-piperidine hydrochloride (1103310-89-9) + 4,4-diphenylbutan-2-one (5409-60-9) → 4-[3-(4-methanesulfonyl-phenyl)-[1,2,4]oxadiazol-5-ylmethyl]-1-(1-methyl-3,3-diphenyl-propyl)-piperidine (1103310-48-0)

Guidance literature:

With sodium tris(acetoxy)borohydride; acetic acid; In dichloromethane; at 20 ℃; for 168h;

Reference yield:

4-[3-(4-methanesulfonyl-phenyl)-[1,2,4]oxadiazol-5-ylmethyl]-piperidine hydrochloride (1103310-89-9) + 2-chloro-ethanol (107-07-3) → 2-(4-[3-(4-methanesulfonyl-phenyl)-[1,2,4]oxadiazol-5-ylmethyl]piperidin-1-yl)-ethanol (1103310-93-5)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; sodium iodide; In acetonitrile; at 150 ℃; for 0.416667h;

upstream raw materials:

4-[3-(4-methanesulfonyl-phenyl)-[1,2,4]oxadiazol-5-ylmethyl]-piperidine-1-carboxylic acid tert-butyl ester

Downstream raw materials:

4-[3-(4-methanesulfonyl-phenyl)-[1,2,4]oxadiazol-5-ylmethyl]-1-(1-methyl-3,3-diphenyl-propyl)-piperidine

2-(4-[3-(4-methanesulfonyl-phenyl)-[1,2,4]oxadiazol-5-ylmethyl]piperidin-1-yl)-ethanol

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