2',3'-O,O-benzylidene adenosine

Base Information

• Chemical Name: 2',3'-O,O-benzylidene adenosine
• CAS No.: 3257-69-0
• Molecular Formula: C₁₇H₁₇N₅O₄
• Molecular Weight: 355.353

Synonyms:2',3'-O,O-benzylidene adenosine

Chemical Property of 2',3'-O,O-benzylidene adenosine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of 2',3'-O,O-benzylidene adenosine

There total 5 articles about 2',3'-O,O-benzylidene adenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

benzaldehyde (100-52-7) + adenosine (58-61-7) → 2',3'-O,O-benzylidene adenosine (3257-69-0)

Guidance literature:

With zinc(II) chloride; at 20 ℃; for 72h; Inert atmosphere;

DOI:10.1016/j.tet.2011.12.011

Reference yield:

C17H16N5O4Pol → 2',3'-O,O-benzylidene adenosine (3257-69-0)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; for 1.5h; solid phase reaction;

DOI:10.1002/ejoc.201200329

Reference yield:

→ O2,O3-Benzyliden-adenosin A (3257-69-0,7721-31-5,32454-65-2,116183-89-2)

Guidance literature:

Adenosin,Benzaldehyd,ZnCl2;

upstream raw materials:

benzaldehyde

adenosine

Downstream raw materials:

4-Sulfamoyl-benzoic acid (3aR,4R,6R,6aR)-6-(6-amino-purin-9-yl)-2-phenyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

4-Phenylsulfamoyl-benzoic acid (3aR,4R,6R,6aR)-6-(6-amino-purin-9-yl)-2-phenyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

4-Benzylsulfamoyl-benzoic acid (3aR,4R,6R,6aR)-6-(6-amino-purin-9-yl)-2-phenyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

4-Phenethylsulfamoyl-benzoic acid (3aR,4R,6R,6aR)-6-(6-amino-purin-9-yl)-2-phenyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

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