N-methyl-2,7-bis[14'-(p-toluenesulfonyl)-3',6',9',12'-tetraoxatetradecyloxycarbonylmethyl]phenothiazine

Base Information

Chemical Name:N-methyl-2,7-bis[14'-(p-toluenesulfonyl)-3',6',9',12'-tetraoxatetradecyloxycarbonylmethyl]phenothiazine
CAS No.:155130-12-4
Molecular Formula:C₅₁H₆₇NO₁₈S₃
Molecular Weight:1078.29
Hs Code.:

Synonyms:N-methyl-2,7-bis[14'-(p-toluenesulfonyl)-3',6',9',12'-tetraoxatetradecyloxycarbonylmethyl]phenothiazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-methyl-2,7-bis[14'-(p-toluenesulfonyl)-3',6',9',12'-tetraoxatetradecyloxycarbonylmethyl]phenothiazine

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Technology Process of N-methyl-2,7-bis[14'-(p-toluenesulfonyl)-3',6',9',12'-tetraoxatetradecyloxycarbonylmethyl]phenothiazine

There total 10 articles about N-methyl-2,7-bis[14'-(p-toluenesulfonyl)-3',6',9',12'-tetraoxatetradecyloxycarbonylmethyl]phenothiazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 155130-07-7
N-methylphenothiazin-2,7-diyldi(acetic acid)

: 155130-15-7
2-[2-[2-[2-(2-hydroxyethoxy)ethoxy]ethoxy]ethoxy]ethyl 4-methylbenzenesulfonate

: 155130-12-4
N-methyl-2,7-bis[14'-(p-toluenesulfonyl)-3',6',9',12'-tetraoxatetradecyloxycarbonylmethyl]phenothiazine

Guidance literature:: With 1,1'-carbonyldiimidazole; methyl trifluoromethanesulfonate; In nitromethane; for 12h;
DOI:10.1002/1099-0690(200109)2001:17<3255::AID-EJOC3255>3.0.CO;2-0

Reference yield:

: 6631-94-3
2-acetylphenothiazine

: 155130-12-4
N-methyl-2,7-bis[14'-(p-toluenesulfonyl)-3',6',9',12'-tetraoxatetradecyloxycarbonylmethyl]phenothiazine

Guidance literature:: Multi-step reaction with 7 steps

1.1: 93 percent / BF₃*OEt₂ / benzene / 36 h / Heating

2.1: n-BuLi / hexane; tetrahydrofuran

3.1: tetrahydrofuran / -40 - 20 °C

4.1: HCl / tetrahydrofuran / 3 h

5.1: 75 percent / AlCl₃ / CS₂ / 14 h / Heating

6.1: S; morpholine / 6 h / Heating

6.2: 97 percent / KOH / H₂O; ethanol / 5 h / Heating

7.1: 60 percent / carbonyldiimidazole; methyl trifluoromethylsulfonate / nitromethane / 12 h

With morpholine; hydrogenchloride; n-butyllithium; aluminium trichloride; boron trifluoride diethyl etherate; sulfur; 1,1'-carbonyldiimidazole; methyl trifluoromethanesulfonate; In tetrahydrofuran; carbon disulfide; nitromethane; hexane; benzene; 5.1: Friedel-Crafts reaction / 6.1: Willgerodt-Kindler reaction;
DOI:10.1002/1099-0690(200109)2001:17<3255::AID-EJOC3255>3.0.CO;2-0

Reference yield:

: 25324-52-1
2-Acetyl-10-methylphenothiazine

: 155130-12-4
N-methyl-2,7-bis[14'-(p-toluenesulfonyl)-3',6',9',12'-tetraoxatetradecyloxycarbonylmethyl]phenothiazine

Guidance literature:: Multi-step reaction with 3 steps

1.1: 75 percent / AlCl₃ / CS₂ / 14 h / Heating

2.1: S; morpholine / 6 h / Heating

2.2: 97 percent / KOH / H₂O; ethanol / 5 h / Heating

3.1: 60 percent / carbonyldiimidazole; methyl trifluoromethylsulfonate / nitromethane / 12 h

With morpholine; aluminium trichloride; sulfur; 1,1'-carbonyldiimidazole; methyl trifluoromethanesulfonate; In carbon disulfide; nitromethane; 1.1: Friedel-Crafts reaction / 2.1: Willgerodt-Kindler reaction;
DOI:10.1002/1099-0690(200109)2001:17<3255::AID-EJOC3255>3.0.CO;2-0