Technology Process of C16H15F3N2O6S
There total 8 articles about C16H15F3N2O6S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine;
In
dichloromethane;
at 0 ℃;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: N-ethyl-N,N-diisopropylamine / 1-methylpiperidin-2-one / -10 - 20 °C
2.1: triethylamine / tetrahydrofuran / 2.67 h / 0 - 20 °C
3.1: ammonium cerium(IV) nitrate / N,N-dimethyl-formamide / 4 h / 0 - 20 °C
4.1: water; iron; ammonium chloride / ethanol / 0.83 h / 100 - 105 °C
5.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C
5.2: 0 - 20 °C
5.3: 2 h / 20 °C
6.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C
6.2: -78 - 20 °C
7.1: triethylamine / dichloromethane / 0 - 20 °C
With
ammonium cerium(IV) nitrate; water; iron; sodium hydride; ammonium chloride; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hexamethyldisilazane;
In
tetrahydrofuran; 1-methylpiperidin-2-one; ethanol; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C
1.2: 0 - 20 °C
1.3: 2 h / 20 °C
2.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C
2.2: -78 - 20 °C
3.1: triethylamine / dichloromethane / 0 - 20 °C
With
sodium hydride; triethylamine; lithium hexamethyldisilazane;
In
tetrahydrofuran; dichloromethane;
