(E)-(S)_s-3-t-butoxycarbonyl-3-p-tolylsulfinylpropenoic acid methyl ester

Base Information

Chemical Name:(E)-(S)_s-3-t-butoxycarbonyl-3-p-tolylsulfinylpropenoic acid methyl ester
CAS No.:133760-94-8
Molecular Formula:C₁₆H₂₀O₅S
Molecular Weight:324.398
Hs Code.:

(E)-(S)<sub>s</sub>-3-t-butoxycarbonyl-3-p-tolylsulfinylpropenoic acid methyl ester

Synonyms:(E)-(S)_s-3-t-butoxycarbonyl-3-p-tolylsulfinylpropenoic acid methyl ester

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Chemical Property of (E)-(S)_s-3-t-butoxycarbonyl-3-p-tolylsulfinylpropenoic acid methyl ester

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Technology Process of (E)-(S)_s-3-t-butoxycarbonyl-3-p-tolylsulfinylpropenoic acid methyl ester

There total 2 articles about (E)-(S)_s-3-t-butoxycarbonyl-3-p-tolylsulfinylpropenoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 133760-93-7
(E)-(S)_s-3-t-butoxycarbonyl-3-p-tolylsulfinylpropenoic acid

: 74-88-4
methyl iodide

: 133760-94-8
(E)-(S)_s-3-t-butoxycarbonyl-3-p-tolylsulfinylpropenoic acid methyl ester

Guidance literature:: With sodium hydrogencarbonate; In N,N-dimethyl-formamide; for 6h; Ambient temperature;
DOI:10.1016/S0957-4166(00)80020-8

Reference yield:

: 58059-08-8
tert-butyl (R)-p-toluenesulfinylacetate

: 133760-94-8
(E)-(S)_s-3-t-butoxycarbonyl-3-p-tolylsulfinylpropenoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / pyrrolidine, triethylamine / dimethylformamide / 24 h / 25 °C

2: 85 percent / NaHCO₃ / dimethylformamide / 6 h / Ambient temperature

With pyrrolidine; sodium hydrogencarbonate; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1016/S0957-4166(00)80020-8