(3aR,3bS,6aR,7aR)-2,2-Dimethyl-tetrahydro-furo[2',3':4,5]furo[2,3-d][1,3]dioxole-5,6-dione 6-(O-benzyl-oxime)

Base Information

Chemical Name:(3aR,3bS,6aR,7aR)-2,2-Dimethyl-tetrahydro-furo[2',3':4,5]furo[2,3-d][1,3]dioxole-5,6-dione 6-(O-benzyl-oxime)
CAS No.:128910-24-7
Molecular Formula:C₁₆H₁₇NO₆
Molecular Weight:319.314
Hs Code.:

Synonyms:(3aR,3bS,6aR,7aR)-2,2-Dimethyl-tetrahydro-furo[2',3':4,5]furo[2,3-d][1,3]dioxole-5,6-dione 6-(O-benzyl-oxime)

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Chemical Property of (3aR,3bS,6aR,7aR)-2,2-Dimethyl-tetrahydro-furo[2',3':4,5]furo[2,3-d][1,3]dioxole-5,6-dione 6-(O-benzyl-oxime)

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Technology Process of (3aR,3bS,6aR,7aR)-2,2-Dimethyl-tetrahydro-furo[2',3':4,5]furo[2,3-d][1,3]dioxole-5,6-dione 6-(O-benzyl-oxime)

There total 1 articles about (3aR,3bS,6aR,7aR)-2,2-Dimethyl-tetrahydro-furo[2',3':4,5]furo[2,3-d][1,3]dioxole-5,6-dione 6-(O-benzyl-oxime) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 22594-19-0
5-hydroxy-1,2-O-isopropylidene-α-D-glucofuranurono-6,3-lactone

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 128910-24-7
(3aR,3bS,6aR,7aR)-2,2-Dimethyl-tetrahydro-furo[2',3':4,5]furo[2,3-d][1,3]dioxole-5,6-dione 6-(O-benzyl-oxime)

Guidance literature:: In benzene; Heating;
DOI:10.1016/0040-4039(90)80078-Z

Reference yield:

: 128910-24-7
(3aR,3bS,6aR,7aR)-2,2-Dimethyl-tetrahydro-furo[2',3':4,5]furo[2,3-d][1,3]dioxole-5,6-dione 6-(O-benzyl-oxime)

: 19130-96-2
1,5-dideoxy-1,5-imino-D-glucitol

Guidance literature:: Multi-step reaction with 4 steps

1: 57 percent / hydrogen / 10 percent Pd/C / ethyl acetate / 2585.7 Torr / Pd(OH)2/C

2: 92 percent / LAH / tetrahydrofuran / 0 °C

3: 90 percent / sat. aq. SO₂ / 35 - 40 °C

4: 75 percent / hydrogen, Ba(OH)2*8H₂O / Raney-Ni / H₂O

With barium dihydroxide; lithium aluminium tetrahydride; sulfur dioxide; hydrogen; palladium on activated charcoal; nickel; In tetrahydrofuran; water; ethyl acetate;
DOI:10.1016/0040-4039(90)80078-Z

Reference yield:

: 128910-24-7
(3aR,3bS,6aR,7aR)-2,2-Dimethyl-tetrahydro-furo[2',3':4,5]furo[2,3-d][1,3]dioxole-5,6-dione 6-(O-benzyl-oxime)

: 123149-59-7,132152-32-0,1196465-02-7
Nojirimycin bisulfite

Guidance literature:: Multi-step reaction with 3 steps

1: 57 percent / hydrogen / 10 percent Pd/C / ethyl acetate / 2585.7 Torr / Pd(OH)2/C

2: 92 percent / LAH / tetrahydrofuran / 0 °C

3: 90 percent / sat. aq. SO₂ / 35 - 40 °C

With lithium aluminium tetrahydride; sulfur dioxide; hydrogen; palladium on activated charcoal; In tetrahydrofuran; ethyl acetate;
DOI:10.1016/0040-4039(90)80078-Z